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33746302030
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1H NMR (CDC13): 7.71 (dd, H5, 3Jnp = 8.6 Hz, 4JHP = 4.4 Hz)). The formation of this product can be explained by a second orfAo-lithiation on the thienyl ring after the rearrangement followed by a nucleophilic attack on the starting S-thienylphosphorothioate 14a. (Figure Presented)
-
1H NMR (CDC13): 7.71 (dd, H5, 3Jnp = 8.6 Hz, 4JHP = 4.4 Hz)). The formation of this product can be explained by a second orfAo-lithiation on the thienyl ring after the rearrangement followed by a nucleophilic attack on the starting S-thienylphosphorothioate 14a. (Figure Presented)
-
-
-
-
71
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33746277591
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For the preparation of diisopropyl phosphorochloridate see
-
For the preparation of diisopropyl phosphorochloridate see:
-
-
-
-
74
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33746312731
-
-
For the preparation of 4,4'-oxydi(benzenethiol) see
-
For the preparation of 4,4'-oxydi(benzenethiol) see:
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