Effect of solution thermodynamics on the purification of two isomorphic steroids by solution crystallization

Chemical Engineering Science

Volumn 61, Issue 18, 2006, Pages 5962-5968

  Nie, Qiang ^a   Wang, Jingkang ^a   Yin, Qiuxiang ^a  

^a TIANJIN UNIVERSITY   (China)

Author keywords

Crystallization; Distribution coefficient; Purity enhancement; Relative solubility; Solid solution

Indexed keywords

CRYSTALLIZATION; HORMONES; PURIFICATION; SOLID SOLUTIONS; SOLUBILITY; SOLVENTS;

CHLOROFORM; DISTRIBUTION COEFFICIENT; PURITY ENHANCEMENT; RELATIVE SOLUBILITY;

DRUG PRODUCTS;

CRYSTALLIZATION; DRUG PRODUCTS; HORMONES; PURIFICATION; SOLID SOLUTIONS; SOLUBILITY; SOLVENTS;

EID: 33746294775     PISSN: 00092509     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ces.2006.05.018     Document Type: Article

References (21)

1. Burton J.A., Prim R.C., and Slichter W.P. Journal of Chemical Physics 21 11 (1953) 1987-1996
2. Charles G., Moyers J.R., and Rousseau R.W. In: Rousseau R.W. (Ed). Handbook of Separation Process Technology (1987), Wiley, New York 578
3. Chernov, A.A, 1984. Modern Crystallography III, Crystal Growth Springer Series On Solid State, vol. 36, Springer, Berlin, p. 179.
4. Ercoli A., De Ruggieri P., and Della Morte D. Gazzetta Chimica Italiana 85 (1955) 628-638
5. Givand J.C., Teja A.S., and Rousseau R.W. A.I.Ch.E. Journal 47 (2001) 2705-2712
6. Givand J.C., Chang B.K., Teja A.S., and Rousseau R.W. Industrial & Engineering Chemistry Research 41 (2002) 1873-1876
7. Meenan P.A., Anderson S.R., and Klug D.L. In: Myerson A.S. (Ed). Handbook of Industrial Crystallization. second ed (2002), Butterworth-Heinemann, Boston 74
8. Nie Q., and Wang J.K. Journal of Chemical and Engineering Data 50 (2005) 1750-1752
9. Nie Q., Wang J.K., Wang Y.L., and Wang S. Journal of Chemical and Engineering Data 50 (2005) 989-992
10. Nie Q., Gong J.B., Wang J.K., and Wang S. Industrial & Engineering Chemistry Research 45 (2006) 432-437
11. Peterson D.H., Meister P.D., Weintraur A., Reineke L.M., Eppstein S.H., Murray H.C., and Leigh Osborn H.M. Journal of the American Chemistry Society 77 (1955) 4428-4429
12. Rosenberger, F., 1979. Fundamentals of Crystal Growth I. Springer, Berlin, pp. 395-493.
13. Rosenberger F., and Riveros H.G. Journal of Chemical Physics 60 (1974) 668-674
14. Teja A.S., Givand J.C., and Rousseau R.W. A.I.Ch.E. Journal 48 (2002) 2629-2634
15. Wang S., Wang Y.L., Nie Q., Zhou L.N., and Wu J.H. Acta Crystallography E60 (2004) o2337-o2338
16. Wang Y.L., Wang S., Hao H.X., Chen W., and Nie Q. Acta Crystallography E60 (2004) o1338-o1339
17. Weiser K. Journal of Physics and Chemistry of Solids 7 (1958) 118-126
18. Wey, J.S., Karpinski, P.H., 2002. Precipitation process. In: Myerson, A.S., (Ed.), Handbook of Industrial Crystallization, second ed. Butterworth-Heinemann, Boston, p. 141.
19. Xu G.Y. Handbook of Intermediate of Pharmaceuticals (2001), Chemical Industry Press, Beijing
20. Yang K., Li X.J., Feng X., Yin Q., and Zhao H.Y. Microbiology 28 (2001) 68-71 (in Chinese)
21. Zhang L.Q., and Zhang M.H. Chinese Pharmaceutical Journal 22 (1987) 7-8