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Synthesis and structural analysis of 5-deoxy-5-[(R,S)-ethylphosphinyl]- α,β-L-idopyranoses
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Structure of nojirimycin, sugar antibiotic with nitrogen in the ring
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0005950519
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Synthesis of 1,2,4-tri-O-acetyl-3,6-di-O-benzyl-5-deoxy-5-C-[(S)- phenylphosphinyl]-β-D-glucopyranose: The first gluco type of hexopyranose derivative having phosphorus in the hemiacetal ring
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(a) Yamamoto, H.; Hosoyamada, C.; Kawamoto, H.; Inokawa, S.; Yamashita, M.; Armour, M.A.; Nakashima, T.T. Synthesis of 1,2,4-tri-O-acetyl-3,6-di-O- benzyl-5-deoxy-5-C-[(S)-phenylphosphinyl]-β-D-glucopyranose: the first gluco type of hexopyranose derivative having phosphorus in the hemiacetal ring. Carbohydr. Res. 1982, 102, 159-167;
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Hanaya, T.; Yamamoto, H. Synthesis and structural analysis of 4-deoxy-4-(hydroxyphosphinyl and phenylphosphinyl)-D-ribofuranoses. Bull. Chem. Soc. Jpn. 1989, 62, 2320-2327.
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14
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33746278629
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note
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1 (no. 33), a = 7.016(4) Å, b = 18.560(5) Å, c = 11.003(4) Å, T = 296 K, Observations [I > 3.00σ(I)] = 847, Variables = 193, Reflection/Parameter ratio = 4.39, R, Rw = 0.067, 0.049. Full crystallographic data (excluding structure factors) have been deposited with the Cambridge Crystallographic Data Center. Copies may be requested free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [fax: +44(0)-1223-336033, or e-mail: deposit@cede.cam.ac.uk].
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15
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33748632563
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On stereochemistry of osmium tetraoxide oxidation of allylic alcohol systems. Empirical rule
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Cha, J.K.1
Christ, W.J.2
Kishi, Y.3
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