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Substrates 1 are readily accessible by 1,6-cuprate addition to 2-en-4-ynoates, see: (a) Krause, N.; Gerold, A. Angew. Chem., Int. Ed. Engl. 1997, 36, 186;
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2 and DMDO furnished product 2b with complete conversion, but in only 38% yield.
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