Synthesis and chiral recognition ability of O-ethyl (2-naphthyl)phosphonothioic acid

Tetrahedron Asymmetry

Volumn 17, Issue 11, 2006, Pages 1617-1621

  Kobayashi, Yuka ^a   Maeda, Jin ^a   Saigo, Kazuhiko ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

O ETHYL (2 NAPHTHYL)PHOSPHONOTHIOIC ACID; THIOACID; UNCLASSIFIED DRUG;

ARTICLE; CHIRALITY; CRYSTALLIZATION; ENANTIOSELECTIVITY; MOLECULAR RECOGNITION; PRIORITY JOURNAL; PURIFICATION; STEREOCHEMISTRY; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 33745834343     PISSN: 09574166     EISSN: 1362511X     Source Type: Journal    
DOI: 10.1016/j.tetasy.2006.06.002     Document Type: Article

References (8)

1. Kobayashi Y., Morisawa F., and Saigo K. Org. Lett. 23 (2004) 4227
2. Kobayashi Y., Morisawa F., and Saigo K. J. Org. Chem. 71 (2005) 606-615
3. Kinbara K., Harada Y., and Saigo K. J. Chem. Soc., Perkin Trans. 2 (2000) 1339
4. Kobayashi Y., Kurasawa T., Kinbara K., and Saigo K. J. Org. Chem. 69 (2004) 7436
5. 2 (4 × 80 mL) and concentration under reduced pressure, gave chemically pure racemic 1 (11.84 g, 47 mmol) in 78% overall yield (on the basis of diethoxyphosphonothioic chloride used).
6. 31P NMR were identical with those of (Sp)-1.
7. 3, Z = 16, R = 0.0510, Rw = 0.0600 (CCDC 605590).
8. 3, Z = 2, R = 0.0430, Rw = 0.0510 (CCDC 605588).