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note
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The reaction of p-toluidine ethylene carbonate and triglyme (solvent) using Na-Y catalyst was carried out at 140 °C for 12 h. The product distribution and progress of the reaction were monitored by withdrawing samples. It was observed that even at lower temperature bis-amino alcohol formation was seen after 70% formation of mono-amino alcohol. It shows that bis-amino alcohol formation is also dependant on the concentration of mono-amino alcohol.
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