Rhodium-catalyzed synthesis of 1-alkynylphosphine oxides from 1-alkynes and tetraphenylbiphosphine

Tetrahedron Letters

Volumn 47, Issue 29, 2006, Pages 5211-5213

  Arisawa, Mieko ^a   Onoda, Masato ^a   Hori, Chieko ^a   Yamaguchi, Masahiko ^a  

^a TOHOKU UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

2,4 DIMETHYLNITROBENZENE; ALKYNE DERIVATIVE; CARBON; NITROBENZENE DERIVATIVE; OXIDE; PHOSPHINE DERIVATIVE; PHOSPHORUS; RHODIUM COMPLEX; TETRAPHENYLBIPHOSPHINE; UNCLASSIFIED DRUG;

ARTICLE; CATALYSIS; CHEMICAL BOND; SYNTHESIS;

EID: 33745060714     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.04.158     Document Type: Article

References (17)

1. Arisawa M., Fujimoto K., Morinaka S., and Yamaguchi M. J. Am. Chem. Soc. 127 (2005) 12226
2. Arisawa M., Ono T., and Yamaguchi M. Tetrahedron Lett. 46 (2005) 5669
3. A review:. Davidsohn W.E., and Henry M.C. Chem. Rev. 67 (1967) 73
4. Also see following examples,. Samb A., Demerseman D., Dixneuf P.H., and Mealli C. Organometallics 7 (1988) 26
5. Galindo A., Mathieu R., Caminade A.-M., and Majoral J.-P. Organometallics 7 (1988) 2198
6. Toyota K., Shibata M., and Yoshifuji M. Bull. Chem. Soc. Jpn. 68 (1995) 2633
7. Corriu R.J.P., Guérin C., Henner B.J.L., and Jolivert A. J. Organomet. Chem. 530 (1997) 39
8. Märkl G., Zollitsch T., Kreitmeier P., Prinzhorn M., Reithinger S., and Eibler E. Chem. Eur. J. 6 (2000) 3806
9. Bharati P., and Periasamy M. Organometallics 19 (2000) 5511
10. Beletskaya I.P., Afanasiev V.V., Kazankova M.A., and Efimova I.V. Org. Lett. 5 (2003) 4309
11. Afanasiev V.V., Beletskaya I.P., Kazankova M.A., Efimova I.V., and Antipin M.U. Synthesis (2003) 2835
12. Mikhailov G.Y., Trostyanskaya I.G., Kazankova M.A., and Lutsenko I.F. J. Gen. Chem. USSR 57 (1987) 2349
13. Angelov C.M., and Neilson R.H. Inorg. Chem. 32 (1993) 334
14. The oxygen atom on 7 may be derived from a small amount of oxygen contaminated.
15. 4, and filtered. After removal of the solvents, flash chromatography (hexane/ethyl acetate = 2/1) over neutral silica gel gave 3 (36.7 mg, 80%) as pale yellow oil.
16. 2: 505.1724. Found: 505.1716.
17. Gaw K.G., Smith M.B., and Slawin A.M.Z. New. J. Chem. 24 (2000) 429