SCOPUS 정보 검색 플랫폼

Volumn 2, Issue 4, 2005, Pages 306-308

A novel route towards the synthesis of stereospecific N-substituted chiral morpholines

Author keywords

Anhydro sugars; Morpholines; Stereospecific synthesis

Indexed keywords

EID: 33744920404 PISSN: 15701786 EISSN: None Source Type: Journal
DOI: 10.2174/1570178054038795 Document Type: Review

Times cited : (8)

References (18)

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18
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- Spectroscopic data of selected compounds; Compound 7: Yellowish solid, mp 111-112°C; (86, α]20D, 34.4° (c, 0. 15, CH2Cl2, 1H NMR (CDCl3, 250 MHz, δ (ppm) 7.24-7.37 (m, 5H, C6H6, 4.89 (d, J-11.7, 1 H, OCHHPh, 4.57 (d, J-11.7, 111, OCHHPh, 4.33 (d, J-6.7, 1H, H-1, 4.24 (dd, J=6.7 and 9.0, 1H, H-2, 4.21 (dd, J=3.1 and 13.0, 1H, H-5, 4.00 (ddd, J=2.7, 10.3, 13.0, 111, NCH2CHHOH, 3.70 (dd, J=4.0 and 8.5, 1H, H-3, 3.64 (ddd, J=3.4, 6.7, 11.7, IH, NCH2CHHOH, 3.35 (dd, J=2.4 and 13.0, 1H, H-5′, 2.71 (ddd, J=2.7, 3.1, 11.7, 1H, NCHHCH2OH, 2.51, bs, 1H, OH, 2.37 (m, 2H, H-4, NCHH CH2OH, 2.31 (s, 3H, NCH3, 13C NMR (CDCl3, 100 MHz, δ (ppm) 42.7 (NCH3, 54.6, NCH2 CH2OH, 60.5 (C-5, 60.7 (C-4, 61.9 O
- 4 (307.39).

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