Effective removal and quantitative analysis of Pd, Cu, Ni, and Pt catalysts from small-molecule products

Synthesis

Volumn , Issue 10, 2006, Pages 1639-1644

  Nielsen, Kim T ^a   Bechgaard, Klaus ^b   Krebs, Frederik C ^a  

^a TECHNICAL UNIVERSITY OF DENMARK   (Denmark)

^b UNIVERSITY OF COPENHAGEN   (Denmark)

Author keywords

Catalysis; Copper; Cross coupling reaction; Nickel; Palladium

Indexed keywords

CHEMICAL ANALYSIS; MOLECULES; NICKEL; PALLADIUM; POLYAMIDES; TRANSITION METALS;

CROSS-COUPLING REACTION; METALLIC FORMS; SOLUBILISATION;

CATALYSTS;

AMIDE; COPPER; METAL; N,N BIS[TETRA(ETHYLENE GLYCOL)MONOMETHYLETHER]PHENYLAZOTHIOFORMAMIDE; N,N DIETHYLPHENYL AZOTHIOFORMAMIDE; NICKEL; PALLADIUM; PLATINUM; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; QUANTITATIVE ANALYSIS; SONOGASHIRA REACTION; SYNTHESIS;

EID: 33744499733     PISSN: 00397881     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2006-926453     Document Type: Article

References (26)

1. Königsberger, K.; Chen, G.; Wu, R. R.; Girgis, M. J.; Prasad, K.; Repič, O.; Blacklock, T. J. Org. Process Res. Dev. 2003, 7, 733.
2. Manley, P. W.; Acemoglu, M.; Marterer, W.; Pachinger, W. Org. Process Res. Dev. 2003, 7, 436.
3. Urawa, Y.; Miyazawa, M.; Ozeki, N.; Ogura, K. Org. Process Res. Dev. 2003, 7, 191.
4. Ferrari, C.; Predieri, G.; Tiripicchio, A. Chem. Mater. 1992, 4, 243.
5. Chen, C.; Dagneau, P.; Grabowski, E. J. J.; Oballa, R.; O'Shea, P.; Prasit, P.; Robichaud, J.; Tillyer, R.; Wang, X. J. Org. Chem. 2003, 68, 2633.
6. Rosso, V. W.; Lust, D. A.; Bernot, O. J.; Grosso, J. A.; Modi, S. P.; Rusowicz, A.; Sedergran, T. C.; Simpson, J. H.; Srivastava, S. K.; Humora, M. J.; Anderson, N. G. Org. Process Res. Dev. 1997, 1, 311.
7. Garret, C. E.; Prasad, K. Adv. Synth. Catal. 2004, 346, 889.
8. Schmuckler, G. (Technion Research and Development Foundation Ltd.), DE1533131, 1974; Chem. Abstr. 1969, 71, 32590.
9. Villa, M.; Cannata, V.; Rosi, A.; Allegrini, P. (Zambon Group S.P.A.) WO 9851646, 1998; Chem. Abstr. 1998, 130, 15127.
10. Krebs, F. C.; Nyberg, R. B.; Jørgensen, M. Chem. Mater. 2004, 16, 1313.
11. Sellinger, A.; Tamaki, R.; Laine, R. M.; Ueno, K.; Tanabe, H.; Williams, E.; Jabbour, G. E. Chem. Commun. 2005, 3700.
12. Nielsen, K. T.; Spanggaard, H.; Krebs, F. C. Macromolecules 2005, 38, 1180.
13. Nielsen, K. T.; Spanggaard, H.; Krebs, F. C. Displays 2004, 25, 231.
14. Nielsen, K. T.; Bechgaard, K.; Krebs, F. C. Macromolecules 2005, 38, 658.
15. Ritleng, V.; Sirlin, C.; Pfeffer, M. Chem. Rev. 2002, 102, 1731.
16. Dieck, H. A.; Heck, F. R. J. Organomet. Chem. 1975, 93, 259.
17. Sonogashira, K.; Tohda, Y.; Hagihara, N. Tetrahedron Lett. 1975, 50, 4467.
18. Milstein, D.; Stille, J. K. J. Am. Chem. Soc. 1978, 100, 3636.
19. Suzuki, A. Acc. Chem. Res. 1982, 15, 178.
20. Negishi, E.; King, A. O.; Okukado, N. J. Org. Chem. 1977, 42, 1821.
21. Okuro, K.; Furuune, M.; Enna, M.; Miura, M.; Nomura, M. J. Org. Chem. 1993, 58, 4716.
22. Beletskaya, I. P.; Latyshev, G. V.; Tsvetkov, A. V.; Lukashev, N. V. Tetrahedron Lett. 2003, 44, 5011.
23. Bechgaard, K. Thesis; University of Copenhagen: Denmark, 1973.
24. Jensen, K. A.; Bechgaard, K.; Pedersen, C. T. H. Acta Chem. Scand. 1972, 26, 2913.
25. Selve, C.; Ravey, J.-C.; Stebe, M.-J.; Moudjahid, C. E.; Moumni, E. M.; Delpuech, J.-J. Tetrahedron 1991, 47, 411.
26. Pedersen, D. S.; Rosenbohm, C. Synthesis 2001, 2431.