Design, construction, and validation of a 1-mm triple-resonance high-temperature-superconducting probe for NMR

Journal of Magnetic Resonance

Volumn 179, Issue 2, 2006, Pages 290-293

  Brey, William W ^a   Edison, Arthur S ^a,b   Nast, Robert E ^c   Rocca, James R ^b   Saha, Saikat ^a   Withers, Richard S ^c  

^a FLORIDA STATE UNIVERSITY   (United States)

^b UNIVERSITY OF FLORIDA   (United States)

^c BRUKER BIOSPIN CORPORATION   (United States)

Author keywords

Biological NMR; Metabolomics; Natural products; Protein screening; Small volume; Superconducting probe

Indexed keywords

MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROBES; PROTEINS; SIGNAL TO NOISE RATIO; SPECTRUM ANALYSIS;

BIOLOGICAL NMR; BRUKER VARIABLE TEMPERATURE; MASS SENSITIVITY; METABOLOMICS; NATURAL PRODUCTS; PROTEIN SCREENING; SMALL VOLUME; Z-AXIS GRADIENT;

SUPERCONDUCTING DEVICES;

IBUPROFEN; UBIQUITIN;

ARTICLE; CHEMISTRY; EQUIPMENT DESIGN; INSTRUMENTATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; TEMPERATURE; VALIDATION STUDY;

EQUIPMENT DESIGN; IBUPROFEN; MAGNETIC RESONANCE SPECTROSCOPY; TEMPERATURE; UBIQUITIN;

EID: 33646473352     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2005.12.008     Document Type: Article

References (13)

1. Hoult D., and Richards R. Signal-to-noise ratio of nuclear magnetic resonance experiment. J. Magn. Reson. 24 (1976) 71-85
2. Olson D.L., Peck T.L., Webb A.G., Magin R.L., and Sweedler J.V. High-resolution microcoil H-l-NMR for mass-limited, nanoliter-vol Samples. Science 270 (1995) 1967-1970
3. Li Y., Logan T.M., Edison A.S., and Webb A.G. Design of small volume HX and triple-resonance probes for improved limits of detection in protein NMR experiments. J. Magn. Reson. 164 (2003) 128-135
4. Kovacs H., Moskau D., and Spraul M. Cryogenically cooled probes - a leap in NMR technology. Prog. NMR Spectrosc. 46 (2005) 131-155
5. Anderson W.A., Brey W.W., Brooke A.L., Cole B., Delin K.A., Fuks L.F., Hill H.D.W., Johanson M.E., Kotsubo V., Nast R., Withers R.S., and Wong W.H. High-sensitivity NMR spectroscopy probe using superconductive coils. Bull. Magn. Reson. 17 (1995) 98-102
6. Hill H.D.W. Improved sensitivity of NMR spectroscopy probes by use of high-temperature superconductive detection coils. IEEE Trans. Appl. Supercon. 7 (1997) 3750-3755
7. W.W. Brey, W. Anderson, W.H. Wong, L.F. Fuks, V.Y. Kotsubo, R.S. Withers, US patent 5,565,778, 1996.
8. Olson D.L., Norcross J.A., O'Neil-Johnson M., Molitor P.F., Detlefsen D.J., Wilson A.G., and Peck T.L. Microflow NMR: concepts and capabilities. Anal. Chem. 76 (2004) 2966-2974
9. Peti W., Norcross J., Eldridge G., and O'Neil-Johnson M. Biomolecular NMR using a microcoil NMR probe-new technique for the chemical shift assignment of aromatic side chains in proteins. J. Am. Chem. Soc. 126 (2004) 5873-5878
10. Corcoran O., and Spraul M. LC-NMR-MS in drug discovery. DDT 8 (2003) 624-631
11. Gronquist M., Meinwald J., Eisner T., and Schroeder F.C. Exploring uncharted terrain in Nature's structure space using capillary NMR spectroscopy: 13 steroids from 50 fireflies. J. Am. Chem. Soc. 127 (2005) 10810-10811
12. Yokoyama S. Protein expression systems for structural genomics and proteomics. Curr. Opin. Chem. Biol. 7 (2003) 39-43
13. Shuker S.B., Hajduk P.J., Meadows R.P., and Fesik S.W. Discovering high-affinity ligands for proteins: SAR by NMR. Science 274 (1996) 1531-1534