A three-dimensional framework structure constructed from 2-(2-pyridyl-N-oxide) ethylphosphonic acid and Nd(III)

Inorganic Chemistry

Volumn 45, Issue 9, 2006, Pages 3741-3745

  Gan, Xin Min ^a   Rapko, Brian M ^a,b   Fox, Jesse ^a   Binyamin, Iris ^a   Pailloux, Sylvie ^a   Duesler, Eileen N ^a   Paine, Robert T ^a  

^a UNIVERSITY OF NEW MEXICO   (United States)

^b PACIFIC NORTHWEST NATIONAL LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33646407561     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic051937+     Document Type: Article

References (35)

1. Clearfield, A. Prog. Inorg. Chem. 1998, 47, 371.
2. Sharma, C. V. K.; Hessheimer, A. J.; Clearfield, A. Polyhedron 2001, 20, 2095.
3. Cao, G.; Lynch, V. M.; Swinnea, J. S.; Mallouk, T. E. Inorg. Chem. 1990, 29, 2112.
4. Wang, R.-C.; Zhang, Y.; Hu, H.-L.; Frausto, R. R.; Clearfield, A. Chem. Mater. 1992, 4, 864.
5. Serpaggi, F.; Ferey, G. J. Mater. Chem. 1998, 8, 2737.
6. Serpaggi, F.; Ferey, G. Inorg. Chem. 1999, 38, 4741.
7. Fanucci, G. E.; Talham, D. R. Langmuir 1999, 15, 3289.
8. Evans, O. R.; Ngo, H. L.; Lin, W. J. Am. Chem. Soc. 2001, 123, 10395.
9. Ngo, H. L.; Lin, W. J. Am. Chem. Soc. 2002, 124, 14298.
10. Song, J.-L.; Lei, C.; Mao, J.-G. Inorg. Chem. 2004, 43, 5630.
11. Clearfield, A.; Sharma, C. V. K.; Zhang, B.-L. Chem. Mater. 2001, 13, 3099.
12. Bligh, S. W. A.; Choi, N.; Geraldes, C. F. G. C.; Knoke, S.; McPartlin, M.; Sanganee, M. J.; Woodroffe, T. M. J. Chem. Soc. Dalton Trans. 1997, 4119.
13. Plutnar, J.; Rohovec, J.; Kotek, J.; Zak, Z.; Lukes, I. Inorg. Chem. Acta 2002, 335, 27.
14. Galdecka, E.; Galdecki, Z.; Gawryszewska, P.; Legendziewicz, J. New J. Chem. 2000, 24, 387.
15. Serre, C.; Stock, N.; Bein, T.; Ferey, G. Inorg. Chem. 2004, 43, 3159.
16. Glowiak, T.; Huskowska, E.; Legendziewicz, J. Polyhedron 1991, 10, 175.
17. Kong, D.; Medvedev, D. G.; Clearfield, A. Inorg. Chem. 2004, 43, 7308.
18. Ayyappan, P.; Evans, O. R.; Foxman, B. M.; Wheeler, K. A.; Warren, T. H.; Lin, W. Inorg. Chem. 2001, 40, 5954.
19. Ayyappan, P.; Evans, O. R.; Cui, Y.; Wheeler, K. A.; Lin, W. Inorg. Chem. 2002, 41, 4978.
20. Kong, D.; Clearfield, A. Cryst. Growth Des. 2005, 5, 1263.
21. De, A. K.; Khopkar, J. M.; Chaliners, R. A. Solvent Extraction of Metals; Van Nostrand-Reinhold: London, 1970.
22. Navratil, J. D.; Schulz, W. W.; Talbot, A. E. Actiniae Recovery from Waste and Low Grade Sources; Harwood Academic: New York, 1982.
23. Actinide/Lanthanide Separations, Choppin, G. R., Navratil, J. D., Schulz, W. W., Eds.; World Scientific: Singapore, 1985.
24. Nash, K. L. Handbook on the Physics and Chemistry of Rare Earths-Lanthanides and Actinides Chemistry; Gschneidner, K. A., Eyring, L. Choppin, G. R., Lander, G. H., Eds.; Elsevier: New York, 1994; Vol. 18.
25. Rapko, B. M.; Duesler, E. N.; Smith, P. H.; Paine, R. T.; Ryan, R. R. Inorg. Chem. 1993, 32, 2164.
26. Gan, X.; Duesler, E. N.; Paine, R. T. Inorg. Chem. 2001, 40, 4420.
27. Nash, K. L.; Lavallette, C.; Borkowski, M.; Paine, R. T.; Gan, X. Inorg. Chem. 2002, 41, 5849.
28. Gan, X.; Binyamin, I.; Rapko, B. M.; Fox, J.; Duesler, E. N.; Paine, R. T. Inorg. Chem. 2004, 43, 2443.
29. Sheldrick, G. M. SHELXL 97; Bruker Instruments: Madison, WI, 1999.
30. 2].
31. Crutchfield, M. M.; Dungen, C. H.; Letcher, J. H.; Mark, V.; VanWazer, J. R. Top. Phosphorus Chem. 1967, 5, 1.
32. Engelhardt, U.; Rapko, B. M.; Duesler, E. N.; Frutos, D.; Paine, R. T. Polyhedron 1995, 14, 2361.
33. Hydrolysis of bis-(trimethylsilyl) phosphonates has been used as a route to other organophosphonic acids: Morita, T.; Okamoto, Y.; Sakurai, H. Bull. Chem. Soc. Jpn. 1978, 51, 2169.
34. -1 M), partially soluble in DMSO, and insoluble in other common organic solvents. Due to the partial solubility in DMSO, some ligand is lost to the DMSO wash phase. These phases can be collected from several syntheses, evaporated, and the residue treated again by aqueous/DMSO workup. This provides for recovery of additional pure acid.
35. 3 (Ln = La, Nd, Eu, Er) colloids and precipitates, as well as thermally aged (100°C, 7 days) hydroxide precipitates.