Discovery of a new polymorph of dehydroepiandrosterone (prasterone) and solution of its crystal structure from X-ray powder diffraction data

Crystal Growth and Design

Volumn 6, Issue 4, 2006, Pages 925-932

  Stahly, G Patrick ^a   Bates, Simon ^a   Andres, Mark C ^a   Cowans, Brett A ^a  

^a SSCI Incorporated   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33646358482     PISSN: 15287483     EISSN: None     Source Type: Journal    
DOI: 10.1021/cg050479c     Document Type: Article

References (14)

1. Kuhnert-Brandstätter, M. Thermomicroscopy in the Analysis of Pharmaceuticals; Pergamon Press: Oxford, 1971.
2. Chang, L.-C.; Caira, C. M. R.; Guillory, J. K. J. Pharm. Sci. 1995, 84, 1169-1179.
3. Caira, M. R.; Guillory, J. K.; Chang, L.-C. J. Chem. Crystallogr. 1995, 25, 393-400.
4. Bhacca, N. S.; Fronczek, F. R.; Sygula, A. J. Chem. Crystallogr. 1996, 26, 483-487.
5. Cox, P. J.; MacManus, S. M.; Gibb, B. C.; Nowell, I. W.; Howie, R. A. Acta Cryst. 1990, C46, 334-336.
6. Frye, J. S.; Maciel, G. E. J. Magn. Reson. 1982, 48, 125-131.
7. Earl, W. L.; VanderHart, D. L. J. Magn. Reson. 1982, 48, 35-54.
8. Pouchert, C. J. The Aldrich Library of NMR Spectra; Aldrich Chemical Co.: Milwaukee, 1983; compound number 12, 578-4.
9. ZOYMOP (FI) and ZOYMOP01 FII.
10. http://www.ing.unitn.it/~luttero/maud/.
11. Patents pending.
12. Gavezzotti, A. Acc. Chem. Res. 1994, 27, 309-314.
13. The pattern indexed is that shown in Figure 3, which was obtained from the sample of FVI provided by Genelabs.
14. DASH, version 2.2; Cambridge Crystallographic Database Centre: Cambridge, UK.