Online flow injection preconcentration and flame atomic absorption spectrometric determination of palladium(II) using inorganic and inorganic-organic hybrid materials-packed microcolumns

Analytical Letters

Volumn 39, Issue 6, 2006, Pages 1187-1199

  Praveen, Ramachandran Sarojam ^a   Daniel, Sobhi ^a   Rao, Talasila Prasada ^a  

^a REGIONAL RESEARCH LABORATORY CSIR   (India)

Author keywords

Atomic absorption spectrometry; C18 bonded silica gel; Diethyl ammonium dithiocarbamate; Dust samples; On line flow injection; Palladium

Indexed keywords

EID: 33646345892     PISSN: 00032719     EISSN: 1532236X     Source Type: Journal    
DOI: 10.1080/00032710600622241     Document Type: Article

References (24)

1. Balcerzak, M. 2000. Analytical chemistry of noble metals. In Encyclopedia of Analytical Chemistry; Meyers, R.A. (ed.); J. Wiley and Sons: Chichester.
2. Begerous, J., Turfeld, M., and Dunemann, L. 1997. Determination of physiological noble metals in human urine using liquid-liquid extraction and Zeeman electrothermal atomic absorption spectrometry. Anal. Chim. Acta, 340: 277-283.
3. Benkhedda, K., Dimitrova, B., Infante, H.G., Ivanova, E., and Adams, F.C. 2003. Simultaneous on-line preconcentration and determination of Pt, Rh and Pd in urine serum and road dust by flow injection combined with inductively coupled plasma time-of-flight mass spectrometry. J. Anal. At. Spectrom., 18: 1019-1025.
4. Eki, L., Soylak, M., Uzun, A., Buyukpatir, E., and Dogan, M. 2000. Determination of trace impurities in some nickel compounds by flame atomic absorption spectrometry after solid phase extraction using Amberlite XAD-16. Fresenius J. Anal. Chem., 368: 358-361.
5. Furhadi, K. and Teimouri, G. 2005. Flame atomic absorption determination of palladium in solutions after preconcentration using octadecyl silica membrane discs modified by thioridazine HCl. Talanta, 65: 925-929.
6. Godlewska-Zylkiewicz, B., Lesniewska, B., Gasiewska, U., and Hulanicki, A. 2000. Ion exchange preconcentration and separation of trace amounts of platinum and palladium. Anal. Lett., 33: 2805-2820.
7. Gomez, M.B. and Palacious, M. A. 2003. ICP-MS determination of Pt, Pd and Rh in airborne and road dust after tellurium coprecipitation. J. Anal. At. Spectrom., 18: 80-83.
8. Jarvis, I., Totland, M.M., and Jarvis, K.E. 1997. Assessment of Dowlex 1-X8-based anion exchange procedures for the separation and determination of ruthenium, rhodium, palladium iridium, platinum and gold in geological samples by inductively coupled plasma mass spectrometry. Analyst, 122: 19-26.
9. Kollenspenger, G., Hann, S., and Stingeder, G. 2000. Determination of Rh, Pd and Pt in environmental silica containing matrices: capabilities and limitations of ICP-MS. J. Anal. At. Spectrom., 15: 1553-1557.
10. Kolthoff, I.M. and Elwing, P.J. 1963. Treatise on Analytical Chemistry, Part II; Vol. 8. Interscience Publishers: New York.
11. Lee, M.L., Tolg, G., Beinrohr, E., and Tschopel, P. 1993. Preconcentration of palladium, platinum and rhodium by on-line sorbent extraction for graphite furnace atomic absorption spectrometry and inductively coupled plasma atomic emission spectrometry. Anal. Chim. Acta, 272: 193-203.
12. Levai, A., Lasztity, A., Zih-Perenyi, K., and Horvath, Zs. 1998. Graphite furnace atomic absorption spectrometry determination and online preconcentration of palladium. Microchem. J., 58: 272-280.
13. Li, C., Chai, C., Mao, X., and Ouyang, H. 1998. Chemical speciation study of platinum group elements in geological samples by stepwise dissolution and inductively coupled plasma mass spectrometry. Anal. Chim. Acta, 374: 93-98.
14. Lin, S., Zhen, Ch., and Yun, G. 1995. Determination of palladium by flame atomic absorption spectrometry combined on-line with flow injection preconcentration using a microcolumn packed with activated carbon fibre. Talanta, 42: 921-926.
15. Meisel, T., Fellner, N., and Mosser, J. 2003. A simple procedure for the determination of platinum group elements and rhenium (Ru, Rh, Pd, Re, Os, Ir and Pt) using ID-ICP-MS with an inexpensive on-line matrix separation in geological and environmental materials. J. Anal. At. Spectrom., 18: 720-726.
16. Moldovan, M., Gomez, M.M., and Palacios, M.A. 2003. On-line preconcentration of palladium on alumina microcolumns and determination in urban waters by ICP-MS. Anal. Chem. Acta, 478: 209-217.
17. Muller, M. and Heumann, K.G. 2000. Isotope dilution inductively coupled plasma quadrupole mass spectrometry in connection with a chromatographic separation for ultra trace determinations of platinum group elements (Pt, Pd, Ru, Ir) in environmental samples. Fresenius J. Anal. Chem., 368: 109-115.
18. Patel, K.S., Sharma, P.C., and Hoffmann, P. 2000. Graphite furnace-atomic absorption spectrophotometric determination of palladium in soil. Fresenius J. Anal. Chem., 367: 738-741.
19. Pyle, J.T. and Jacobs, W.D. 1964. Solvent extraction of platinum and palladium with derivatives of dithiocarbamate acid. Anal. Chem., 36: 1686-1799.
20. Rauch, S., Motelica-Hieno, M., Morrison, G.M., and Donard, O.F.X. 2000. Critical assessment of platinum group element determination in road and urban river sediments using ultrasonic nebulisation and high resolution ICP-MS. J. Anal. At. Spectrom., 15: 329-334.
21. Ravindra, K., Bencs, L., and VanGrieken, R. 2004. Platinum group elements in the environment and their health risk. Sci. Total Environ., 318: 1-43.
22. Schuster, M. and Shwarzer, M. 1996. Selective determination of palladium by online column preconcentration and graphite furnace atomic absorption spectrometry. Anal. Chem. Acta, 328: 1-11.
23. Tilch, J., Ludke, C., and Hoffmann, E. 1996. Determination of metals in airborne particulates by LEAFS and ICP-MS after sampling on reusable graphite filters. Fresenius J. Anal. Chem., 355: 913-915.
24. Valsankova, R., Otruba, V., Bendl, J., Fisera, M., and Kanicky, V. 1999. Preconcentration of platinum group metals on modified silica gel and their determination by inductively coupled plasma-atomic emission spectrometry and inductively coupled plasma mass spectrometry in air borne particulate. Talanta, 48: 839-846.