Reaction of S2CC(PPh3)2 with silver salts containing weakly coordinating anions; preparation and crystal structures of [Ag6{S2CC(PPh3)2} 4][BF4]6 and [Ag4 {S2CC(PPh3)2}4] [Al{OC(CF3)3}4] 4

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 632, Issue 5, 2006, Pages 859-865

  Petz, Wolfgang ^a   Neumüller, Bernhard ^a   Krossing, Ingo ^b  

^a PHILIPPS UNIVERSITY MARBURG   (Germany)

^b BCH 3307   (Switzerland)

Author keywords

Argentophilic interactions; Betain like compounds; Carbodiphosphorane CS2 adduct; Crystal structures; Silver cluster compounds

Indexed keywords

EID: 33646254624     PISSN: 00442313     EISSN: 15213749     Source Type: Journal    
DOI: 10.1002/zaac.200500477     Document Type: Article

References (50)

1. a) C. N. Matthews, J. S. Driscoll, G. H. Birum, J. Chem. Soc., Chem. Commun. 1966, 736.
2. b) C. N. Matthews, G. H. Birum, Tetrahedron Lett. 1966, 46, 5707.
3. a) F. Ramirez, J. F. Pilot, N. B. Desai, C. B. Smith, B. Hansen, N. McKelvie, J. Am. Chem. Soc. 1967, 89, 6273.
4. b) F. K. Ross, W. C. Hamilton, F. Ramirez, Acta Crystallogr. 1971, 527, 2331.
5. a) H. Schmidbaur, C. E. Zybill, D. Neugebauer, Angew. Chem. 1982, 94, 321;
6. Angew. Chem., Int. Ed. Engl. 1982, 21, 310.
7. b) H. Schmidbaur, C. Zybill, D. Neugebauer, G. Müller, Z. Naturforsch. 1985, 40b, 1293.
8. c) W. Petz, C. Kutschera, S. Tschan, F. Weller, B. Neumüller, Z. Anorg. Allg. Chem. 2003, 629, 1235.
9. a) W. Petz, F. Weller, J. Uddin, G. Frenking, Organometallics 1999, /5, 619 (Ni).
10. b) J. Sundermeyer, K. Weber, K. Peters, H. G. von Schnering, Organometallics 1994, 13, 2560 (Re).
11. c) H. Schmidbaur, C. E. Zybill, G. Müller, C. Krüger, Angew. Chem. 1983, 95, 753;
12. Angew. Chem., Int. Ed. Engl. 1983, 22, 729 (Cu).
13. d) J. Vicente, A. R. Singhal, P. G. Jones, Organometallics 2002, 21, 5887 (Au).
14. W. Petz, C. Kutschera, M. Heitbaum, G. Frenking, R. Tonner, B. Neumüller, Inorg. Chem. 2005, 44, 1263.
15. W. Petz, B. Neumüller, unpublished results.
16. M. A. Rawashdeh-Omary, M. A. Omary, H. H. Patterson, J. Am. Chem. Soc. 2000, 122, 10371.
17. a) H. Schmidbaur, Chem. Soc. Rev. 1995, 24, 443.
18. b) F. Scherbaum, A. Grohmann, B. Huber, C. Krüger, H. Schmidbaur, Angew. Chem. 1988, 100, 1542;
19. Angew. Chem., Int. Ed. Engl. 1988, 27, 1544.
20. c) H. Schmidbaur, W. Graf, G. Müller, Angew. Chem. 1988, 100, 439;
21. Angew. Chem., Int. Ed. Engl. 1988, 27, 417.
22. a) P. Pyykkö, F. Mendizabal, Inorg. Chem. 1998, 37, 3018.
23. b) A. Codina, E. J. Fernandez, P. G. Jones, A. Laguna, J. M. Lopez-de-Luzuriaga, M. Monge, M. E. Olmos, J. Perez, M. A. Rodriguez, J. Am. Chem. Soc. 2002, 124, 6781, and literature therein.
24. I. Krossing, Chem. Eur. J. 2001, 7, 490.
25. th Ed., Clarendon Press, Oxford, 1984.
26. b) J. Emsley, The Elements, Clarendon, Oxford, 1989, p. 174.
27. B. Djordjevic, O. Schuster, H. Schmidbaur, Inorg. Chem. 2005, 44, 673.
28. G. Henkel, P. Betz, B. Krebs, Angew. Chem. 1987, 99, 131;
29. Angew. Chem., Int. Ed. Engl. 1987, 26, 145.
30. B. Noren, A. Oskarson, Acta Chem. Scand., Ser. A, 1985, 39, 701.
31. J. A. Schuermann, F. R. Fronczek, J. Selbin, Inorg. Chim. Acta 1989, 160, 43.
32. V. J. Catalano, M. A. Malwitz, Inorg. Chem. 2003, 42, 5483.
33. J. C. Garrison, R. S. Simons, W. G. Kofron, C. A. Tessier, W. J. Youngs, J. Chem. Soc., Chem. Commun. 2001, 1780.
34. a) D. A. Edwards, R. M. Harker, M. F. Mahon, K. C. Molloy, J. Chem. Soc., Dalton Trans. 1997, 3509.
35. b) P. M. Jeffries, S. R. Wilson, G. S. Girolami, J. Organomet. Chem. 1993, 449, 203.
36. c) E. M. Meyer, S. Gambrotta, C. Floriani, A. Chiesi-Villa, C. Guastini, Organometallics 1989, 8, 1067.
37. d) S. Gambrotta, C. Floriani, A. Chiesi-Villa, C. Guastini, J. Chem. Soc., Chem. Commun. 1983, 1087.
38. e) A. N. Nesmeyanov, N. N. Sedova, Yu. T. Struchkov, V. G. Andrianov, E. N. Stakheeva, V. A. Sazonova, J. Organomet. Chem. 1978, 153, 115.
39. P. Römbke, A. Schier, H. Schmidbaur, S. Cronje, H. Raubenheimer, Inorg. Chim. Acta 2004, 357, 235.
40. a) D. Fenske, T. Langetepe, Angew. Chem. 2002, 114, 306;
41. Angew. Chem., Int. Ed. Engl. 2002, 41, 300.
42. b) S. Canales, O. Crespo, M. C. Gimeno, P. G. Jones, A. Laguna, A. Silvestru, Inorg. Chim. Acta 2003, 347, 16.
43. c) M. G. Kanatzidis, Song-Ping Huang, Angew. Chem. 1989, 101, 1556;
44. Angew. Chem., Int. Ed. Engl. 1989, 28, 1513.
45. d) Xiang-Lin Jin, Ka-Luo Tang, Yao-Ling Long, Yu Liang, You-Qi Tang, Gaodeng Xuexiao Huaxue (Chin.) (Chem. J. Chin. Uni.) 1999, 20, 831.
46. Jin Zhao, D. Adcock, W. T. Pennington, J. W. Kolis, Inorg. Chem. 1990, 29, 4358.
47. Yong-Yue Lin, Siu-Wai Lai, Chi-Ming Che, Kung-Kai Cheung, Zhong-Yuan Zhou, Organometallics 2002, 21, 2275.
48. G. M. Sheldrick, SHELXTL-Plus, Release 4.2 for Siemens Crystallographic Systems R3, Siemens Analytical X-Ray Instruments Inc., Madison (WI), 1990.
49. G. M. Sheldrick, SHELXS-97, Programm zur Lösung von Kristallstrukturen, Göttingen 1997.
50. G. M. Sheldrick, SHELXH-97, Universität Göttingen 1997.