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33646152708
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note
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3Cu: Found: C, 32.0; H, 1.1; N, 33.3%. Calc.: C, 32.2; H, 1.2; N, 33.4%.
-
-
-
-
13
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33646160163
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note
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2) = 0.0707, S = 1.032. A crystal was mounted on Lindemann-glass capillaries and transferred into the cold nitrogen stream of a Nonius KappaCCD diffractometer on rotating anode (Mo Kα radiation, graphite monochromator, λ = 0.71073 Å). The intensity data were corrected for Lorentz and polarisation effects, for absorption and extinction. The structures were solved by direct methods. The programs COLLECT [20], SHELXS-97 [21], SHELXL-97 [22] were used for data reduction, structure solution and structure refinement, respectively. All non-hydrogen atoms were refined anisotropically. All H atoms were introduced in calculated positions and refined with fixed geometry with respect to their carrier atoms. Crystallographic data for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary Publication No. CCDC-295012. Copies of available material can be obtained, free of charge, on application to the Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: +44 0 1223 336 033 or e-mail: deposit@ccdc.cam.ac.uk).
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18
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33646158423
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note
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-1). X-band EPR spectra were recorded on polycrystalline samples at RT at 77 K with a Jeol RE2X electron spin resonance spectrometer using DPPH (g = 2.0036) as a standard.
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20
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0004182772
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Nonius BV, Delft, The Netherlands
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Nonius. COLLECT (2002), Nonius BV, Delft, The Netherlands
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COLLECT
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Nonius1
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23
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0003625968
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Wilkinson G., Gillard R.D., and McCleverty J.A. (Eds), Pergamon Press, Oxford, UK
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van Albada, G.A.1
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0035952315
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Kooijman H., Spek A.L., van Albada G.A., Gamez P., and Reedijk J. Acta Cryst. C 60 (2004) m51
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