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Volumn 9, Issue 5, 2006, Pages 441-443

A rare 2D structure of a novel Cu(II) dinuclear-based compound with dicyanamide and 4-nitropyridine-N-oxide as ligands

Author keywords

2D structure; Copper; Dicyanamide; Nitropyridine

Indexed keywords


EID: 33646133451     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2006.02.006     Document Type: Article
Times cited : (13)

References (26)
  • 12
    • 33646152708 scopus 로고    scopus 로고
    • note
    • 3Cu: Found: C, 32.0; H, 1.1; N, 33.3%. Calc.: C, 32.2; H, 1.2; N, 33.4%.
  • 13
    • 33646160163 scopus 로고    scopus 로고
    • note
    • 2) = 0.0707, S = 1.032. A crystal was mounted on Lindemann-glass capillaries and transferred into the cold nitrogen stream of a Nonius KappaCCD diffractometer on rotating anode (Mo Kα radiation, graphite monochromator, λ = 0.71073 Å). The intensity data were corrected for Lorentz and polarisation effects, for absorption and extinction. The structures were solved by direct methods. The programs COLLECT [20], SHELXS-97 [21], SHELXL-97 [22] were used for data reduction, structure solution and structure refinement, respectively. All non-hydrogen atoms were refined anisotropically. All H atoms were introduced in calculated positions and refined with fixed geometry with respect to their carrier atoms. Crystallographic data for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary Publication No. CCDC-295012. Copies of available material can be obtained, free of charge, on application to the Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: +44 0 1223 336 033 or e-mail: deposit@ccdc.cam.ac.uk).
  • 18
    • 33646158423 scopus 로고    scopus 로고
    • note
    • -1). X-band EPR spectra were recorded on polycrystalline samples at RT at 77 K with a Jeol RE2X electron spin resonance spectrometer using DPPH (g = 2.0036) as a standard.
  • 20
    • 0004182772 scopus 로고    scopus 로고
    • Nonius BV, Delft, The Netherlands
    • Nonius. COLLECT (2002), Nonius BV, Delft, The Netherlands
    • (2002) COLLECT
    • Nonius1
  • 23
    • 0003625968 scopus 로고
    • Wilkinson G., Gillard R.D., and McCleverty J.A. (Eds), Pergamon Press, Oxford, UK
    • Hathaway B.J. In: Wilkinson G., Gillard R.D., and McCleverty J.A. (Eds). Comprehensive Coordination Chemistry vol. 5 (1987), Pergamon Press, Oxford, UK
    • (1987) Comprehensive Coordination Chemistry , vol.5
    • Hathaway, B.J.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.