Influence of synthetic routes on the conformational order and mobility of C18 and C30 stationary phases

Journal of Chromatography A

Volumn 1113, Issue 1-2, 2006, Pages 45-54

  Srinivasan, Gokulakrishnan ^a   Meyer, Christoph ^b   Welsch, Norbert ^b   Albert, Klaus ^b   Müller, Klaus ^a  

^a UNIVERSITY OF STUTTGART   (Germany)

^b UNIVERSITY OF TÜBINGEN   (Germany)

Author keywords

Alkyl chain lengths; C18; C30 alkyl modified silica gels; Conformational order; FTIR; HPLC; Mobility; NMR; Synthetic routes

Indexed keywords

CROSSLINKING; FOURIER TRANSFORM INFRARED SPECTROSCOPY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOMERS; MOLECULAR STRUCTURE; SILANES; SILICA GEL;

ALKYL CHAIN LENGTHS; C18; C30 ALKYL MODIFIED SILICA GELS; CONFORMATIONAL ORDER; MOBILITY; SYNTHETIC ROUTES;

CONFORMATIONS;

ALKYL GROUP; CARBON; CARBON 18; CARBON 30; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; CHEMICAL STRUCTURE; CONFORMATIONAL TRANSITION; CROSS LINKING; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INFRARED SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; STRUCTURE ANALYSIS; SYNTHESIS;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR CONFORMATION; SPECTROSCOPY, FOURIER TRANSFORM INFRARED;

EID: 33645974906     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2006.01.113     Document Type: Article

References (45)

1. Vansant E.F., VanDerVoort P., and Vrancken K.C. Characterization and Chemical Modification of the Silica Surface (1995), Elsevier, Amsterdam
2. Neue U.D. In: Meyers R.A. (Ed). Encylopedia of Analytical Chemistry (2000), Wiley, Chichester
3. Doyle C.A., and Dorsey J.G. In: Katz E., Eksteen R., Schoenmakers P., and Miller N. (Eds). The Handbook of Liquid Chromatography (1998), Marcel Dekker, New York 293
4. Sander L.C., Lippa K.A., and Wise S.A. Anal. Bioanal. Chem. 382 (2005) 646
5. Saito Y., Ohta H., and Jinno K. J. Sep. Sci. 26 (2003) 225
6. Sentell K.B. J. Chromatogr. A 656 (1993) 231
7. Nawrocki J., Dunlap C.J., Carr P.W., and Blackwell J.A. Biotechnol. Prog. 10 (1994) 561
8. Pesek J.J., and Matyska M.T. In: Cases J. (Ed). Encylopedia of Chromatography (2001), Marcel Dekker, New York
9. Sander L.C., and Wise S.A. J. Chromatogr. A 656 (1993) 335
10. Sander L.C., Pursch M., and Wise S.A. Anal. Chem. 71 (1999) 4821
11. Unger K.K. Porous Silica (1979), Elsevier, Amsterdam
12. Nawrocki J., Rigney M.P., McCormick A., and Carr P.W. J. Chromatogr. A 657 (1993) 229
13. Pursch M., Sander L.C., and Albert K. Anal. Chem. 68 (1996) 4107
14. Rimmer C.A., Sander L.C., Wise S.A., and Dorsey J.G. J. Chromatogr. A 1007 (2003) 11
15. Pursch M., Strohschein S., Handel H., and Albert K. Anal. Chem. 68 (1996) 386
16. Sander L.C., and Wise S.A. J. Sep. Sci. 24 (2001) 910
17. Tchapla A., Heron S., Lesellier E., and Colin H. J. Chromatogr. A 656 (1993) 81
18. Schunk T.C., and Burke M.F. J. Chromatogr. A 656 (1993) 289
19. Sander L.C., Callis J.B., and Field L.R. Anal. Chem. 55 (1983) 1068
20. Singh S., Wegmann J., Albert K., and Müller K. J. Phys. Chem. B 106 (2002) 878
21. Srinivasan G., Pursch M., Sander L.C., and Müller K. Langmuir 20 (2004) 1746
22. Srinivasan G., Kyrlidis A., McNeff C., and Müller K. J. Chromatogr. A 1081 (2005) 132
23. Srinivasan G., Neumann-Singh S., and Müller K. J. Chromatogr. A 1074 (2005) 31
24. Srinivasan G., Sander L.C., and Müller K. Anal. Bioanal. Chem. 384 (2006) 514
25. Doyle C.A., Vickers T.J., Mann C.K., and Dorsey J.G. J. Chromatogr. A 877 (2000) 25
26. Doyle C.A., Vickers T.J., Mann C.K., and Dorsey J.G. J. Chromatogr. A 877 (2000) 41
27. Ducey M.W., Orendorff C.J., Pemberton J.E., and Sander L.C. Anal. Chem. 74 (2002) 5585
28. Ducey M.W., Orendorff C.J., Pemberton J.E., and Sander L.C. Anal. Chem. 74 (2002) 5576
29. Pursch M., Brindle R., Ellwanger A., Sander L.C., Bell C.M., Handel H., and Albert K. Solid State Nucl. Magn. Reson. 9 (1997) 191
30. Pursch M., Sander L.C., and Albert K. Anal. Chem. News Features 71 (1999) 733A
31. Pursch M., Vanderhart D.L., Sander L.C., Gu X., Nguyen T., Wise S.A., and Gajewski D.A. J. Am. Chem. Soc. 122 (2000) 6997
32. Neumann-Singh S., Villanueva-Garibay J., and Müller K. J. Phys. Chem. B 108 (2004) 1906
33. Sander L.C., Sharpless K.E., Craft N., and Wise S.A. Anal. Chem. 66 (1994) 1667
34. Emenhiser C., Sander L.C., and Schwartz S.J. J. Chromotogr. A 707 (1995) 205
35. Emenhiser C., Englert G.E., Sander L.C., Ludwig B., and Schwartz S.J. J. Chromatogr. A 719 (1996) 333
36. Wegmann J., Albert K., Pursch M., and Sander L.C. Anal. Chem. 73 (2001) 1814
37. Meyer C., Skogsberg U., Welsch N., and Albert K. Anal. Bioanal. Chem. 382 (2005) 679
38. Sander L.C., and Wise S.A. Anal. Chem. 67 (1995) 3284
39. Raitza M., Pursch M., Strohschein S., Albert K., and Sander L.C. GIT Lab. J. 2 (1998) 237
40. SRM 869, Column Selectivity Test Mixture for Liquid Chromatography (Polycyclic Aromatic Hydrocarbons), Certificate of Analysis, US National Institute of Standards and Technology (NIST), Gaithersburg, MD, 1998.
41. Wirth M.J., and Fatumbi H.O. Anal. Chem. 65 (1993) 822
42. Strohschein S., Pursch M., and Albert K. J. Pharm. Biomed. Anal. 21 (1999) 669
43. Albert K., Schmid J., Pfleiderer B., and Bayer E. In: Mottola H.A., and Steinmetz J.R. (Eds). Chemically Modified Surfaces (1992), Elsevier, Amsterdam 105
44. Tonelli A.E. Spectroscopy and Polymer Microstructure (1989), The Conformational Connection VCH, New York
45. Snyder R.G., Strauss H.L., and Elliger C.A. J. Phys. Chem. 86 (1982) 5145