Syntheses and X-ray structures of base-stabilized iminoalanes

Organometallics

Volumn 25, Issue 6, 2006, Pages 1392-1398

  Schulz, Stephan ^a   Thomas, Florian ^b   Priesmann, Wolfgang M ^b   Nieger, Martin ^b  

^a UNIVERSITY OF PADERBORN   (Germany)

^b UNIVERSITY OF BONN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

MONOMERS; NUCLEAR MAGNETIC RESONANCE; SPECTROSCOPIC ANALYSIS; STRUCTURE (COMPOSITION); X RAY ANALYSIS;

BASE-STABILIZED IMINOALANES; DIHYDROANTHRACENE;

NITROGEN COMPOUNDS;

EID: 33645451788     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om0509286     Document Type: Article

References (35)

1. Hudlicky, M. In Reductions in Organic Chemistry, 2nd ed.; American Chemical Society: Washington, DC, 1996.
2. Wiberg, E.; May, A. Z. Naturforsch. B 1955, 10, 229.
3. See the following and references therein: (a) Chang, C.-C.; Ameerunisha, M. S. Coord. Chem. Rev. 1999, 189, 199.
4. (b) Bauer, T.; Schulz, S.; Hupfer, H.; Nieger, M. Organometallics 2002, 21, 2931.
5. (a) Veith, M. Chem. Rev. 1990, 90, 3.
6. (b) Perego, G.; del Piero, G.; Cesari, M.; Zazzetta, A.; Dozzi, G. J. Organomet. Chem. 1975, 87, 53.
7. (c) del Piero, G.; Cesari, M.; Dozzi, G.; Mazzei, A. J. Organomet. Chem. 1977, 129, 281.
8. (d) Cesari, M.; Perego, G.; del Piero, G.; Cucinella, S.; Cernia, E. J. Organomet. Chem. 1974, 78, 203.
9. (e) del Piero, G.; Perego, G.; Cucinella, S.; Cesari, M.; Mazzei, A. J. Organomet. Chem. 1977, 136, 13.
10. (f) Perego, G.; Dozzi, G. J. Organomet. Chem. 1981, 205, 21.
11. (g) Perego, G.; Cesari, M.; del Piero, G.; Balducci, A.; Cernia, E. J. Organomet. Chem. 1975, 87, 33.
12. (h) del Piero, G.; Cucinella, S.; Cesari, M. J. Organomet. Chem. 1979, 173, 263.
13. (i) Harlan, C. J.; Bott, S. G.; Barron, A. R. J. Chem. Soc., Dalton Trans. 1997, 637.
14. Hardman, N. J.; Cui, C.; Roesky, H. W.; Fink, W. H.; Power, P. P. Angew. Chem., Int. Ed. 2001, 40, 2172.
15. (a) Schulz, S.; Häming, L.; Herbst-Irmer, R.; Roesky, H. W.; Sheldrick, G. M. Angew. Chem., Int. Ed. Engl. 1994, 33, 969.
16. (b) Fisher, J. D.; Shapiro, P. J.; Yap, G. P. A.; Rheingold, A. L. Inorg. Chem. 1996, 35, 271.
17. (c) Wehmschulte, R. J.; Power, P. P. J. Am. Chem. Soc. 1996, 118, 791.
18. (d) Schulz, S.; Voigt, A.; Roesky, H. W.; Häming, L.; Herbst-Irmer, R. Organometallics 1996, 15, 5252.
19. (e) Wehmschulte, R. J.; Power, P. P. Inorg. Chem. 1998, 37, 6906.
20. (f) Uhl, W.; Molter, J.; Koch, R. Eur. J. Inorg. Chem. 1999, 2021.
21. (a) Wagonner, K. M.; Hope, H.; Power, P. P. Angew. Chem., Int. Ed. 1988, 27, 1699.
22. (b) Wagonner, K. M.; Power, P. P. J Am. Chem. Soc. 1991, 113, 3385.
23. Hamilton, T. P.; Shaikh, A. W. Inorg. Chem. 1997, 36, 754.
24. See for instance: Power, P. P. Chem. Rev. 1999, 99, 3463.
25. 13C NMR spectra of some compounds could not be recorded due to their poor solubility in organic solvents.
26. Thomas, F.; Bauer, T.; Schulz, S.; Nieger, M. Z. Anorg. Allg. Chem. 2003, 629, 2018.
27. (a) Vedejs, E.; Chen, X. J. Am. Chem. Soc. 1996, 118, 1809.
28. (b) Cuperly, D.; Gros, P.; Fort, Y. J. Org. Chem. 2002, 67, 238.
29. (a) Schulz, S.; Nieger M. Organometallics 2000, 19, 2640.
30. (b) Schulz, S.; Thomas, F.; Kuczkowski, A.; Hupfer, H.; Nieger M. Organometallics 2000, 19, 5758.
31. (c) Thomas, F.; Schulz, S.; Nieger, M. Eur. J. Inorg. Chem. 2001, 161.
32. Schulz, S.; Roesky, H. W.; Koch, H. J.; Sheldrick, G. M.; Stalke, D.; Kuhn, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1729.
33. Moberg, C.; Adolfson, H. In Catalysis 1: Organometallics, Vol. 4: Compounds of Group 15 (As, Sb, Bi) and Silicon Compounts; Flemming, I. (Hrsg.); Science of Synthesis: Houben-Weyl, Methods of Molecular Transformations, Thieme, 2001.
34. Sheldrick, G. M. SHELXS-97, Program for Structure Solution: Acta Crystallogr. Sect. A 1990, 46, 467.
35. Sheldrick, G. M. SHELXL-97, Program for Crystal Structure Refinement; Universität Göttingen, 1997.