Iodobenzene diacetate on alumina: Efficient synthesis of 1,3,4-oxadiazolyl-1,8-naphthyridines in solventless system using microwaves

Journal of Heterocyclic Chemistry

Volumn 43, Issue 2, 2006, Pages 485-488

  Mogilaiah, K ^a   Rani, J Uma ^a   Sakram, B ^a   Reddy, N Vasudeva ^a  

^a KAKATIYA UNIVERSITY   (India)

Author keywords

[No Author keywords available]

Indexed keywords

1,3,4 OXADIAZOLYL 1,8 NAPHTHYRIDINE; [2 OXO 2 (4 METHOXYPHENYL) 2H [1,8]NAPHTHYRIDIN 1 YL]ACETIC ACID HYDRAZIDE; ACETOACETIC ACID; ALUMINUM OXIDE; HYDRAZIDE DERIVATIVE; IODOBENZENE DIACETATE; NAPHTHYRIDINE DERIVATIVE; SOLVENT; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; MICROWAVE RADIATION; OXIDATION; REACTION ANALYSIS; SYNTHESIS;

EID: 33645242651     PISSN: 0022152X     EISSN: None     Source Type: Journal    
DOI: 10.1002/jhet.5570430235     Document Type: Article

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17. IBD (0.355 g, 10.0 mmol) per gram of neutral alumina is ground using a pestle and mortar; the recovered alumina after removal of the products is reused without any loss of activity.
18. The design involves piercing the roof of a domestic microwave oven and as such, proper sealing must be done in order to avoid the hazards of direct microwave exposure to the investigator.