Capillary electrophoretic analysis of phosphorus species in clandestine methamphetamine laboratory samples

Journal of Forensic Sciences

Volumn 51, Issue 1, 2006, Pages 82-86

  Knops, Lori A ^a   Northrop, David M ^b,d   Person, Eric C ^c  

^a N Carolina State Bur of Invest   (United States)

^b Washington State Patrol   (United States)

^c CALIFORNIA STATE UNIVERSITY   (United States)

^d Washington State Patrol   (United States)

Author keywords

Capillary electrophoresis; Dynamically coated capillaries; Forensic science; Hypophosphite; Hypophosphorous acid; Manufacture; Methamphetamine; Phosphate; Phosphite; Phosphorus

Indexed keywords

ACETIC ACID; AZIDE; BROMIDE; CARBONIC ACID; CHLORATE; CHLORIDE; CHROMIC ACID; FLUORIDE; ILLICIT DRUG; IODIDE; IODINE; METHAMPHETAMINE; NITRATE; NITRITE; PERCHLORATE; PHOSPHATE; PHOSPHITE; PHOSPHORUS; SULFATE; SULFITE; THIOCYANATE;

ADSORPTION; ANALYTIC METHOD; ARTICLE; CAPILLARY ELECTROPHORESIS; DRUG DETERMINATION; DRUG TRAFFIC; MATERIAL COATING; PRIORITY JOURNAL; SEPARATION TECHNIQUE; TEMPERATURE;

EID: 33645217945     PISSN: 00221198     EISSN: 15564029     Source Type: Journal    
DOI: 10.1111/j.1556-4029.2005.00007.x     Document Type: Article

References (29)

1. Ely RA McGrath DC. Lithium-ammonia reduction of ephedrine to methamphetamine an unusual clandestine synthesis. J Forensic Sci 1990 35 3 720 3.
2. Skinner HF. Methamphetamine synthesis via hydriodic acid/red phosphorus reduction of ephedrine. Forensic Sci Int 1990 48 123 34.
3. Federal Register notice control of red phosphorus, white phosphorus, and hypophosphorous acid (and its salts) as List 1 chemicals. J Clandestine Lab Invest Chem Assoc (law enforcement restricted) 2002 12 1 11 6.
4. Skoog DA Leary JJ. Principles of instrumental analysis. 4th ed. Orlando, FL Saunders College Publishing 1992.
5. Schieferecke J Worley D. Analysis of red phosphorus using a pyrolysis gas chromatograph/mass spectrometer. J Anal Appl Pyrolysis 2004 71 1 47 50.
6. McKibben TD. Analyses of inorganic components found in clandestine drug laboratory evidence. J Clandestine Lab Invest Chem Assoc (law enforcement restricted) 1995 5 4 19 33.
7. McKibben TD. Rapid color/precipitation test for hypophosphorous acid and salts. Abstracts of the Eleventh Annual CLIC Technical Training Seminar; 2001 September 4-8; Monterey, CA.
8. Kato N Sakayanagi M Nakayama T Nishimura H. Detection of multiple anions by thin-layer chromatography. J Chromatogr A 2002 973 159 66.
9. Christian DR. Ammonium molybdate crystal test for phosphorus. J Clandestine Lab Invest Chem Assoc (law enforcement restricted) 1997 7 4 28 9.
10. Romano J Jandik P Jones WR Jackson PE. Optimization of inorganic capillary electrophoresis for the analysis of anionic solutes in real samples. J Chromatogr A 1991 546 411 21.
11. Gebauer P Deml M Bocek P Janák J. Determination of nitrate, chloride and sulphate in drinking water by capillary free-zone electrophoresis. J Chromatogr A 1983 267 455 7.
12. Lurie IS. The analysis of cations and anions in illicit heroin using capillary electrophoresis with indirect UV detection. J Capillary Electrophor 1996 3 5 237 42.
13. Huang X Luckey JA Gordon MJ Zare RN. Quantitative analysis of low molecular weight carboxylic acids by capillary zone electrophoresis/conductivity detection. Anal Chem 1989 61 7 766 70.
14. Northrop DM. Gunshot residue analysis by micellar electrokinetic capillary electrophoresis assessment for application to casework. Part II. J Forensic Sci 2001 46 3 560 72.
15. Northrop DM McCord BR Butler JM. Forensic applications of capillary electrophoresis. J Capillary Electrophor 1994 1 2 158 68.
16. Northrop DM MacCrehan WA Martire DE. Separation and identification of organic gunshot and explosive constituents by micellar electrokinetic capillary electrophoresis (MECE). Anal Chem 1991 63 1038 42.
17. McCord BR Hargadon KA Hall KE Burmeister SG. Forensic analysis of explosives using ion chromatographic methods. Anal Chim Acta 1994 288 43 56.
18. Weinberger R Lurie IS. Micellar electrokinetic capillary chromatography of illicit drug substances. Anal Chem 1991 63 823 7.
19. Bokor I Trenerry VC Scheelings P. Separation and quantitation of optical isomers of methylamphetamine samples by capillary electrophoresis. Forensic Sci Int 1997 85 177 92.
20. Foret F Fanali S Ossicini L Bocek P. Indirect photometric detection in capillary zone electrophoresis. J Chromatogr A 1989 470 299 308.
21. Person EC Knops LA. Clandestine ammonia generation. J Clandestine Lab Invest Chem Assoc (law enforcement restricted) 2004 14 1 20 7.
22. Janssens J Chevigne R Louis P inventors. Analis SA, assignee. Capillary electrophoresis method using initialized capillary and polyanion-containing buffer and chemical kit. US patent 5,611,903. March 22, 1995.
23. Lurie IS Hays PA Parker K. Capillary electrophoresis analysis of a wide variety of seized drugs using the same capillary with dynamic coatings. Electrophoresis 2004 25 1580 91.
24. Lurie IS Bethea MJ McKibben TD Hays PA Pellegrini P Sahai R Garcia AD Weinberger R. Use of dynamically coated capillaries for the routine analysis of methamphetamine, amphetamine, MDA, MDMA, MDEA, and cocaine using capillary electrophoresis. J Forensic Sci 2001 46 5 1025 32.
25. Vallely PB. A single step process for methamphetamine manufacture using hypophosphorous acid. J Clandestine Lab Invest Chem Assoc (law enforcement restricted) 1995 5 2 14 5.
26. Willers LJ. The detection of phosphine gas produced from hydriodic acid and the evaluation of detection instruments for use in clandestine laboratory environments. J Clandestine Lab Invest Chem Assoc (law enforcement restricted) 2003 13 2 14 24.
27. Skinner HF Oulton SR. Identification and quantitation of hydriodic acid manufactured from iodine, red phosphorus and water. J Clandestine Lab Invest Chem Assoc (law enforcement restricted) 1995 5 4 12 8.
28. Beveridge A. editor. Forensic investigation of explosions. Bristol, PA Taylor & Francis Inc. 1998.
29. Yinon J Zitrin S. Modern methods and applications in analysis of explosives. Chichester, West Sussex, England John Wiley & Sons 1993.