Synthesis and characterization of Nitro-p-xylenes

Molecules

Volumn 10, Issue 8, 2005, Pages 978-989

  Yan Hong, Liu ^a   Tong Lai, Zhang ^a   Jian Guo, Zhang ^a   Jin Yu, Guo ^a   Kai Bei, Yu ^b  

^a BEIJING INSTITUTE OF TECHNOLOGY   (China)

^b INSTITUTE OF GEOLOGY AND GEOPHYSICS   (China)

Author keywords

Nitration; p Xylene; Thermal Analysis

Indexed keywords

XYLENE;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; DIFFERENTIAL SCANNING CALORIMETRY; INFRARED SPECTROPHOTOMETRY; SYNTHESIS; TEMPERATURE; X RAY CRYSTALLOGRAPHY;

CALORIMETRY, DIFFERENTIAL SCANNING; CRYSTALLOGRAPHY, X-RAY; MODELS, MOLECULAR; SPECTROPHOTOMETRY, INFRARED; TEMPERATURE; XYLENES;

EID: 33644808304     PISSN: 14203049     EISSN: 14203049     Source Type: Journal    
DOI: 10.3390/10080978     Document Type: Article

References (17)

1. Guisnet, M.; Gnep, N. S.; Morin, S. Micropor. Mesopor. Mat. 2000, 35-36, 47-59
2. Aboul-Gheit, A. K.; Abdel-Hamid, S. M.; Emam, E. A. Catalytic para-xylene maximization alkylation of toluene with methanol on platinum loaded zeolite catalysts prepared via different routes. Appl. Catal. A: Gen. 1999, 179, 107-115.
3. Glinzer, E.; Fitting, R. Ann. 1865, 136, 307-308.
4. Nolting, E.; Forel, S. Ber. 1885, 18, 2680.
5. Konowalow, M.; Gurewitsch, Ch. J. Russ. Phys. Chem. Soc. 1905, 27,537-41;
6. [Chem. Zentr., 1905, 76, II, 818].
7. Batchelder, G. W.; Nagle, W.M.; Vyverberg, J.C.; Willis, J. M. U.S. Patent No. 2,400,904, 1946.
8. Lellmann, E. Ann. 1885, 228, 250-3.
9. Giua, M. Gazz. Chim. Ital. 1919, 49, 149.
10. Davis, T. L. "Chemistry of Powder and Explosives"; John Wiley. & Sons: New York, 1941; pp. 133-5, 141-150
11. Groggins, P.H. "Unit Processes in Organic Synthesis"; McGraw-Hill Book Co.: New York, 1947; pp. 48-51
12. Shipp, K.G.; Kaplan, L.A. Reaction of a substituted polynitrotoluene II. The generation and reactions of 2,4,6-trinitrobenzylanion, J. Org. Chem. 1966, 31, 857.
13. Atkin, R.L.; Hollins, R.A.; Wilson, W.S. Synthesis of polynitro compounds. Hexasubstituted benzenes, J. Org. Chem. 1986, 51, 3261-3266.
14. CCDC number 258942 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/ conts/retrieving.html (or from the CCDC, 12 Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033; e-mail: deposit@ccdc.cam.ac.uk).
15. Sheldrick, G. M. SHELXS98 Program for the Solution of Crystal Structure; University of Gottingen: Gottingen, Germany; 1998.
16. Liu, Y.; Zhang, T.; Zhang, J.; Guo, J.; Yu, K. Preparation, Structural Characterization and the Molecular Structure of 2,3,5-trinitro-p-xylene. Struct. Chem. in press.
17. Groggins, P. H. "Unit Processes in Organic Synthesis"; McGraw-Hill Book Co.: New York, 1947; p. 25.