Segmental orientation of thermoplastic polyurethanes investigated by 1H double-quantum NMR. Correlation with thermodynamic and mechanical properties

Polymer

Volumn 47, Issue 6, 2006, Pages 2069-2079

  Voda, Alexandra ^a,b   Voda, Mihai A ^b   Beck, Klaus ^a   Schauber, Thomas ^a   Adler, Matthias ^a   Dabisch, Thomas ^c   Bescher, Martin ^a   Viol, Michael ^d   Demco, Dan E ^b   Blümich, Bernhard ^b  

^a Bei Freudenberg Forschungsdienste KG   (Germany)

^b RWTH AACHEN UNIVERSITY   (Germany)

^c Merkel Freudenberg Fluidtechnic GmbH   (Germany)

^d Technisches Entwicklungszentrum   (Germany)

Author keywords

1H double quantum NMR; Residual dipolar couplings; Thermoplastic polyurethane

Indexed keywords

MOLECULAR WEIGHT; NUCLEAR MAGNETIC RESONANCE; QUANTUM THEORY; THERMODYNAMICS;

1H DOUBLE-QUANTUM NMR; RESIDUAL DIPOLAR COUPLINGS; THERMOPLASTIC POLYURETHANE;

POLYURETHANES;

MOLECULAR WEIGHT; POLYURETHANE; THERMODYNAMICS; THERMOPLASTIC POLYMER; YOUNG MODULUS;

EID: 33644764839     PISSN: 00323861     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.polymer.2006.01.023     Document Type: Article

References (32)

1. J.P. Cohen Addad Prog NMR Spectrosc 25 1993 1 312
2. D.E. Demco, S. Hafner, and H.W. Spiess V.M. Litvinov P.P. De Handbook of spectroscopy of rubbery materials 2002 Rapra Technology Ltd Shawbury
3. D.E. Demco, and B. Blümich Encycl Polym Sci Technol 10 2004 637 685
4. M. Schneider, L. Gasper, D.E. Demco, and B. Blümich J Chem Phys 111 1999 402 415
5. R. Fechete, D.E. Demco, and B. Blümich Macromolecules 35 2002 6083 6085
6. M. Wang, M. Bertmer, D.E. Demco, B. Blümich, V.M. Litvinov, and H. Barthel Macromolecules 36 2003 4411 4413
7. M. Voda, D.E. Demco, J. Perlo, R.A. Orza, and B. Blümich J Magn Reson 172 2005 98 109
8. R.S. Maxwell, and B. Balazs J Chem Phys 116 2002 10492 10502
9. K. Saalwächter, P. Ziegler, O. Spyckerelle, B. Haidar, A. Vidal, and J.-U. Sommer J Chem Phys 116 2003 3468 3478
10. K. Saalwächter J Am Chem Soc 125 2003 14684 14685
11. A. Wiesmath, C. Filip, D.E. Demco, and B. Blümich J Magn Reson 149 2001 258 263
12. A. Wiesmath, C. Filip, D.E. Demco, and B. Blümich J Magn Reson 154 2002 60 72
13. V.M. Litinov, M. Bertmer, L. Gasper, D.E. Demco, and B. Blümich Macromolecules 36 2003 7598 7606
14. M. Bertmer, L. Gasper, D.E. Demco, B. Blümich, and V.M. Litvinov Macromol Chem Phys 205 2004 83 94
15. T-F. Hsu, and Y.-D. Lee Polymer 40 1999 577 587
16. A. Kretschmer, R. Drake, M. Neidhoefer, and M. Wilhelm Solid State Nucl Magn Reson 22 2002 204 217
17. D.Sh. Idiyatullin, E.V. Khozina, and V.S. Smirnov Solid State Nucl Magn Reson 7 1996 17 26
18. Voda A, Beck K, Schauber T, Adler M, Dabisch T, Bescher M, et al. Polym Test. In press.
19. M.C. Show, and G.J. DeSalvo On the plastic flow beneath a blunt axisymmetric intender Trans ASME 92 1970
20. T.L. Smith J Polym Sci Phys 12 1974 1825 1835
21. M.D. Lelah, and S.L. Cooper Polyurethanes in medicine 1953 CRC Press Boca Raton, FL
22. S. Gopakumar, C.I. Paul, and M.R. Gopinathan Nair Mater Sci (Poland) 23 2005 227 232
23. R.F. Story, and C.D. Hoffmann Polymer 33 1992 2807 2816
24. J.C. West, and S.L. Cooper Science and technology of rubber 1978 Academic Press New York
25. R.J. Young Introduction to polymers 1983 University Press Cambridge
26. G. Wegner Termoplastic elastomers 1st ed 1987 Carl Hansen Munich
27. D. Roylance Yield and plastic flow 2002 Massachusetts Institute of Technology, Department of Materials Science Engineering
28. M.C.E.I. Niesten, and R.J. Gaymans Polymer 42 2001 6199 6207
29. M. Doi, and S.F. Edwards The theory of polymer dynamics 1986 Clarendon Press Oxford
30. M. Rubinstein, and R. Colby Polymer physics 2003 University Press Oxford
31. A-N. Gent Engineering with rubber 1992 Carl Hanser Munich
32. A.V. Tobolsky Properties and structure of polymers 1960 Wiley New York, USA