Isolation and quantitation of amygdalin in Apricot-kernel and Prunus Tomentosa Thunb. by HPLC with solid-phase extraction

Journal of Chromatographic Science

Volumn 43, Issue 7, 2005, Pages 383-387

  Lv, Wei Feng ^a   Ding, Ming Yu ^a   Zheng, Rui ^a  

^a TSINGHUA UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

PRUNUS; PRUNUS ARMENIACA; PRUNUS TOMENTOSA;

AMYGDALIN; CARBON NANOTUBE;

ARTICLE; CHEMISTRY; FRACTIONATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOLATION AND PURIFICATION; METHODOLOGY; PLANT SEED; PRUNUS;

AMYGDALIN; CHEMICAL FRACTIONATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; NANOTUBES, CARBON; PRUNUS; SEEDS;

EID: 32944459373     PISSN: 00219665     EISSN: 00219665     Source Type: Journal    
DOI: 10.1093/chromsci/43.7.383     Document Type: Article

References (13)

1. Pharmacopoeia Committee of P.R. China. Pharmacopoeia of P.R. China Part I, 2000 edition. Chemical Industry Press, Beijing, China, 2000, pp. 160-61.
2. Pharmacopoeia Committee of P.R. China. Pharmacopoeia of P.R. China Part I, 2000 edition. Chemical Industry Press, Beijing, China, 2000, pp.166-67.
3. T. Isozaki, Y. Matano, K. Yamamoto, N. Kosaka, and T. Tani. Quantitative determination of amygdalin epimers by cyclodextrin-modified micellar electrokinetic chromatography. J. Chromatogr. A 923: 249-54 (2001).
4. K.N. Syrigos, B.G. Rowlinson, and A.A. Epenetos. In vitro cytotoxicity following specific activation of amygdalin by beta-glucosidase conjugated to a bladder cancer-associated monoclonal antibody. Int. J. Cancer 78: 712-19 (1998).
5. P. Zhen, D.B. Wang, T.J. Jia, and X.M. Bai. Analysis on amygdalin of Prunus Tomentosa Thunb. by HPLC. J. Zhangjiakou TCM. Coll. 19: 13-14 (2002).
6. S. Ma and C.H. Li. Determination of amygdalin in Apricot-kernel. Chin. J. Exp. Trad. Med. Form. 6: 16-17 (2000).
7. E.Y. Hwang, J.H. Lee, Y.M. Lee, and S.P. Hong. Reverse-phase HPLC separation of D-amygdalin and neoamygdalin and optimum conditions for inhibition of racemization of amygdalin. Chem. Pharm. Bull. 50: 1373-75 (2002).
8. E.Y. Hwang, S.S. Lee, J.H. Lee, and S.P. Hong. Development of quantitative extraction method of amygdalin without enzymatic hydrolysis from Tonin(Persicae Semen) by high performance liquid chromatography. Arch. Pharm. Res. 25: 453-56 (2002).
9. K. Wasserkrug and Z. ElRassi. High-performance liquid phase separation of glycosides. 1. Reversed phase chromatography of cyanogenic glycosides with uv and pulsed amperometric detection. J. Liq. Chromatogr. Related Technol. 20: 335-49 (1997).
10. T. Cirns, J. Froberg, and S. Gonzales. Analytical chemistry of amygdalin. Anal. Chem. 50: 317-22 (1978).
11. P. Louchouarn, S. Opsahl, and R. Benner. Isolation and quantification of dissolved lignin from natural waters using solid-phase extraction and GC/MS. Anal. Chem. 72: 2780-87 (2000).
12. J.P. Lai, X.W. He, Y. Jiang, and F. Chen. Preparative separation and determination of matrine from the Chinese medicinal plant Sophora flavescens Ait by molecularly imprinted solid-phase extraction. Anal. Bioanal. Chem. 375: 264-69 (2003).
13. Y.Q. Cai, G.B. Jiang, J.F. Liu, and Q.X. Zhou. Multiwalled carbon nanotubes as a solid-phase extraction adsorbent for the determination of bisphenol a, 4-n-nonylphenol, and 4-tert-octylphenol. Anal. Chem. 75: 2517-21 (2003).