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59
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32644469265
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note
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3CN with 0.1% TFA and 99.9% water with 0.1% TFA. The separation gradient was 0-100% organic over 15 min, 100% organic for 10 min, and 100-0% organic over 1 min. Samples were run over at a constant flow rate of 1 mL/min and a temperature of 30°C. Detection was at 254 nm.
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60
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32644458360
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note
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+].
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