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32644448437
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-1; R(F) = 3.63%, wR(F) = 7.89%.
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17
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37049096497
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τ = (β - α)/60, where β is the largest angle and α is the second-largest angle in the coordination sphere. See: Addison, A. W.; Rao, T. N. J. Chem. Soc., Dalton Trans. 1984, 1349.
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32644442056
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note
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-1; R(F) = 6.84%, wR(F) = 17.20%. Selected bond lengths (Å) and angles (deg): Ga-O1 = 1.867(3), Ga-O2 = 1.833(3), Ga-O3 = 1.839(3), Ga-N1 = 2.092(4), Ga-N2 = 2.172(3), O1-Ga-N2 = 165.78(13), O2-Ga-O3 = 112.98(12), O2-Ga-N1 = 131.81(13), O3-Ga-N1 = 114.84-(14), N1-Ga-N2 = 80.42(13), O2-Ga-N2 = 91.39(12), O3-Ga-N2 = 93.32(12), N1-Ga-O1 = 87.68(13), O2-Ga-O1 = 90.78(12), O3-Ga-O1 = 98.76(13).
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