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7 (5, 20.5 g, 63.4 mmol), and stirred for 1 day at ambient temperature. The color of solution turned to brown, then filtered and hydrolysis by dilute hydrochloric acid. The organic phase was extracted with ether, and volatile material was removed in vacuo. Kuger-Rohr distillation (200°C, 0.01 mmHg) gave colorless crystals of 1 (2.60mg, 5.98 mmol) in 19% yield.
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