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Volumn 47, Issue 11, 2006, Pages 1849-1852

Synthesis of naphtho[b]cyclobutenes from 1,2-bis(3-propynol)benzenes

Author keywords

2+2 Cycloaddition; Bisallenes; Dephosphinylation; Naphtho b cyclobutenes

Indexed keywords

ALCOHOL DERIVATIVE; BENZENE DERIVATIVE; CYCLOBUTANE DERIVATIVE; PHOSPHINE DERIVATIVE;

EID: 32244440573     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2005.12.121     Document Type: Article
Times cited : (15)

References (30)
  • 6
    • 0030005845 scopus 로고    scopus 로고
    • Production of 9a from 6 was described in the review article by Grissom (J.W. Grissom, G.U. Gunawardena, D. Klingberg, and D. Huang Tetrahedron 52 1996 6453 6518 ). However, no original manuscript dealing with the details of this reaction is available
    • (1996) Tetrahedron , vol.52 , pp. 6453-6518
    • Grissom, J.W.1    Gunawardena, G.U.2    Klingberg, D.3    Huang, D.4
  • 7
    • 32244436967 scopus 로고    scopus 로고
    • note
    • 2O: C, 76.72; H, 5.19. Found: C, 76.78; H, 5.30.
  • 8
    • 24944584108 scopus 로고    scopus 로고
    • N. Krause A.S.K. Hashmi Wiley-VCH Weinheim
    • For the preparation of allenes via the [2,3]-sigmatropic rearrangement of propargyl phosphinites, see: A.S.K. Hashmi N. Krause A.S.K. Hashmi Modern Allene Chemistry Vol. 1 2004 Wiley-VCH Weinheim 3 50
    • (2004) Modern Allene Chemistry , vol.1 , pp. 3-50
    • Hashmi, A.S.K.1
  • 19
    • 32244443169 scopus 로고    scopus 로고
    • note
    • Substrates were prepared by one- or two-step Sonogashira coupling of diiodobenzene with substituted propargyl alcohols.
  • 24
    • 32244443282 scopus 로고    scopus 로고
    • note
    • 4, and concentrated. Chromatography of the residue with hexane afforded 16 (32.3 mg, 70%) as a colorless solid.
  • 29
    • 0002234399 scopus 로고
    • 2 reagent is effective for reduction of alkene, alkynes, and halides: E.C. Ashby, and J.J. Lin Tetrahedron Lett. 1977 4481 4484
    • (1977) Tetrahedron Lett. , pp. 4481-4484
    • Ashby, E.C.1    Lin, J.J.2
  • 30
    • 32244438321 scopus 로고    scopus 로고
    • note
    • The diastereomer ratio of 14c was as same as that of 18.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.