Determination of N-nitroso derivatives of hexahydro-1,3,5-trinitro-1,3,5- triazine (RDX) in soils by pressurized liquid extraction and liquid chromatography-electrospray ionization mass spectrometry

Journal of Chromatography A

Volumn 1107, Issue 1-2, 2006, Pages 2-8

  Pan, Xiaoping ^a   Zhang, Baohong ^a   Cox, Stephen B ^a   Anderson, Todd A ^a   Cobb, George P ^a  

^a TEXAS TECH UNIVERSITY   (United States)

Author keywords

DNX; ElectroSpray ionization (ESI); Explosives; Liquid chromatography (LC); Mass spectrometry (MS); MNX; N Nitroso compounds (NOCs); Pressurized liquid extraction (PLE); RDX; Soil; TNX

Indexed keywords

DERIVATIVES; EXPLOSIVES; EXTRACTION; IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; SOILS; TOXICITY;

DNX; ELECTROSPRAY IONIZATION (ESI); MNX; N-NITROSO COMPOUNDS (NOC); PRESSURIZED LIQUID EXTRACTION (PLE); RDX; TNX;

NITROGEN COMPOUNDS;

ACETIC ACID; ACETONITRILE; CYCLONITE; HEXAHYDRO 1 NITROSO 3,5 DINITRO 1,3,5 TRIAZINE; HEXAHYDRO 1,3 DINITROSO 5 NITRO 1,3,5 TRIAZINE; HEXAHYDRO 1,3,5 TRINITROSO 1,3,5 TRIAZINE; MAGNESIUM TRISILICATE; NITROSO DERIVATIVE; TRIAZINE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; ELECTROSPRAY MASS SPECTROMETRY; LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; REPRODUCIBILITY; SANDY LOAM; SOIL; SOLVENT EXTRACTION;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; NITROSO COMPOUNDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOIL POLLUTANTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TRIAZINES;

EISENIA FETIDA;

EID: 31844432366     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2005.12.025     Document Type: Article

References (28)

1. J.L. Davis, A.H. Wani, B.R. O'Neal, and L.D. Hansen J. Hazard. Mater. B 112 2004 45
2. M.E. Walsh, T.F. Jenkins, Indetification of TNT Transformation Products in Soil, Technical report CRREL-SR-92-16, Cold Regions Research Engineering Laboratory, Hanover, NH, 1992.
3. Health advisory for RDX, US Environmental Protection Agency, Washington, DC, 1988.
4. P.M. Lish, B.S. Levine, E.M. Furedi-Machacek, E.M. Sagartz, V.S. Rac, Determination of the chronic mammalian toxicological effects of RDX: 24 month chronic toxicity/carcinogenicity study of hexahydro-1,3,5-trinitro-1,3,5- triazine (RDX) in the B6C3F1 hybrid mouse, US Army Medical Research and Development Command, Doc Number AD A 160774, 1984.
5. C.L. Kitts, D.P. Cunningham, and P.J. Unkefer Appl. Environ. Microbiol. 60 1994 4608
6. D.M. Young, C.L. Kitts, P.J. Unkefer, and K.L. Ogden Biotechnol. Bioeng. 56 1997 258
7. N.R. Adrian, and C.M. Arnett Curr. Microbiol. 48 2004 332
8. B. Bhushan, A. Halasz, S. Thiboutot, G. Ampleman, and J. Hawari Biochem. Biophys. Res. Commun. 316 2004 816
9. N.G. McCormick, J.H. Cornell, and A.M. Kaplan Appl. Environ. Microbiol. 42 1981 817
10. H.R. Beller Environ. Sci. Technol. 36 2002 2060
11. R. Gray, R. Peto, P. Brantom, and P. Grasso Cancer Res. 51 1991 6470
12. B.H. Zhang, P.N. Smith, and T.A. Anderson J. Chromatogr. A 1101 2006 38
13. B.H. Zhang, R.J. Kendall, T.A. Anderson, Chemospere, in press.
14. J.N. Smith, X.P. Pan, A. Gentles, E.E. Smith, S.B. Cox, G.P. Cobb, Environ. Toxicol. Chem. 25, in press.
15. D.S. Moore Rev. Sci. Instrum. 75 2004 2499
16. T.F. Jenkins, M.E. Walsh, P.W. Schumacher, P.H. Miyares, C.F. Bauer, and C.L. Grant J. AOAC 72 1989 890
17. Method 8330, Nitroaromatics and nitramines by High Performance Liquid Chromatography (HPLC), http://www.epa.gov/epaoswer/hazwaste/test/pdfs/8330.pdf, US Environmental Protection Agency, 1994.
18. S. Campbell, R. Ogoshi, G. Uehara, and Q.X. Li J. Chromatogr. Sci. 41 2003 284
19. X.P. Pan, B.H. Zhang, and G.P. Gobb Talanta 67 2005 816
20. B.H. Zhang, X.P. Pan, G.P. Cobb, and T.A. Anderson J. Chromatogr. B 824 2005 277
21. D.W. Berberich, R.A. Yost, and D.D. Fetterolf J. Forensic Sci. 33 1988 946
22. T.M. Chow, M.R. Wilcoxon, M.D. Piwoni, and N.R. Adrian J. Chromatogr. Sci. 42 2004 470
23. X. Zhao, and J. Yinon J. Chromatogr. A 977 2002 59
24. C.A. Groom, A. Halasz, L. Paquet, S. Thiboutot, G. Ampleman, and J. Hawari J. Chromatogr. A 1072 2005 73
25. E. Holmgren, H. Carlsson, P. Goede, and C. Crescenzi J. Chromatogr. A 1099 2005 127
26. SW846 Test Methods SW846, US Environmental Protection Agency, Washington, DC, 2000.
27. D.L. Kaplan S.K. Sikdar R.L. Irvine Bioremediation: Principles and Practice, Vol. II, Biodegradation Technology Developments 1988 Technomic Publications Lancaster, PA 549 575
28. J. Hawari, A. Halasz, T. Sheremata, S. Beaudet, C. Groom, L. Paquet, C. Rhofir, G. Ampleman, and S. Thiboutot Appl. Environ. Microbiol. 66 2000 2652