Controlled hydrolysis reactions of the group 15 element-azamacrocyclic complexes MCl3L (M = As, Sb or Bi; L = 1,4,7-trimethyl-1,4,7-triazacyclononane). Formation and crystal structures of

Journal of the Chemical Society - Dalton Transactions

Volumn , Issue 21, 1996, Pages 4045-4053

  Willey, Gerald R ^a   Daly, Leo T ^a   Meehan, Paul R ^a   Drew, Michael G B ^b  

^a UNIVERSITY OF WARWICK   (United Kingdom)

^b UNIVERSITY OF READING   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 31644436407     PISSN: 03009246     EISSN: None     Source Type: Journal    
DOI: 10.1039/DT9960004045     Document Type: Article

References (44)

1. G. R. Willey, L. T. Daly, M. D. Rudd and M. G. B. Drew, Polyhedron, 1995, 14, 315.
2. (a) E. Hough, D. G. Nicholson and A. K. Vasudevan, J. Chem. Soc., Dalton Trans., 1987, 427;
3. (b) N. W. Alcock, M. Ravindran and G. R. Willey, J. Chem. Soc., Chem. Commun., 1989, 1063;
4. M. G. B. Drew, D. G. Nicholson, I. Sylte and A. Vasudevan, Inorg. Chim. Acta, 1990, 171, 11;
5. (d) N. W. Alcock, M. Ravindran, S. M. Roe and G. R. Willey, Inorg. Chim. Acta, 1990, 167, 115;
6. (e) B. Beagley, M. Endregard and D. G. Nicholson, Acta Chem. Scand., 1991, 45, 439;
7. (f) M. Schafer, G. Frenzen, B. Neumüller and K. Dehnicke, Angew. Chem., Int. Ed. Engl., 1992, 31, 334;
8. (g) R. Garbe, B. Vollmer, B. Neumüller, J. Pebler and K. Dehnicke, Z. Anorg. Allg. Chem., 1993, 619, 271;
9. (h) R. D. Rogers, A. H. Bond, S. Aguinaga and A. Reyes, J. Am. Chem. Soc., 1992, 114, 2967;
10. (i) N. W. Alcock, M. Ravindran and G. R. Willey, Acta Crystallogr., Sect. B, 1993, 49, 507;
11. (j) H. v. Arnim, K. Dehnicke, K. Maczek and D. Fenske, Z. Naturforsch., Teil B, 1993, 48, 1331.
12. G. R. Willey, M. T. Lakin, M. Ravindran and N. W. Alcock, J. Chem. Soc., Chem. Commun., 1991, 271;
13. G. R. Willey, M. T. Lakin and N. W. Alcock, J. Chem. Soc., Dalton Trans., 1992, 591; 1339.
14. G. R. Willey, A. Asab, M. T. Lakin and N. W. Alcock, J. Chem. Soc., Dalton Trans., 1993, 365.
15. K. Wieghardt, M. Kleine-Boymann, B. Nuber and J. Weiss, Inorg. Chem., 1986, 25, 1654.
16. M. Walter and L. Ramaley, Anal. Chem., 1973, 45, 165.
17. T. J. Atkins, J. E. Richman and W. F. Oettle, Org. Synth., 1978, 58, 86;
18. (b) D. W. White, B. A. Karcher, R. A. Jacobson and J. G. Verkade, J. Am. Chem. Soc., 1979, 101, 4921;
19. K. Wieghardt, P. Chaudhuri, B. Nuber and J. Weiss, Inorg. Chem., 1982, 21, 3086.
20. W. Kabsch, J. Appl. Crystallogr., 1988, 21, 916.
21. SHELXS 86, G. M. Sheldrick, Acta Crystallogr., Sect. A, 1990, 46, 467.
22. N. Walker and D. Stuart, Acta Crystallogr., Sect. A, 1983, 39, 158.
23. G. M. Sheldrick, SHELXL 93, Program for crystal structure refinement, University of Göttingen, 1993.
24. A. Neuhaus, G. Frenzen, J. Pebler and K. Dehnicke, Z. Anorg. Allg. Chem., 1992, 618, 93.
25. G. R. Willey, M. P. Spry and M. G. B. Drew, Polyhedron, 1996, 15, 4497.
26. M. R. Churchill, A. G. Landers and A. L. Rheingold, Inorg. Chem., 1981, 20, 849.
27. M. Hall and D. B. Sowerby, J. Chem. Soc., Chem. Commun., 1979, 1134;
28. M. Hall, M. Nunn, M. J. Begley and D. B. Sowerby, J. Chem. Soc., Dalton Trans., 1986, 1231.
29. R. D. Rogers and M. L. Jezl, Acta Crystallogr., Sect. C, 1994, 50, 1527.
30. A. L. Rheingold, A. G. Landers, P. Dahlstrom and J. Zubieta, J. Chem. Soc., Chem. Commun., 1979, 143.
31. R. Yang and L. J. Zompa, Inorg. Chem., 1976, 15, 1499.
32. C. F. G. C. Geraldes, M. C. Alpoim, M. P. M. Marques, A. D. Sherry and M. Singh, Inorg. Chem., 1985, 24, 3876.
33. K. Wieghardt, S. Brodka, K. Peters, E. M. Peters and A. Simon, Z. Naturforsch., Teil B, 1987, 42, 279.
34. See for example, P. Chaudhuri and K. Wieghardt, Prog. Inorg. Chem., 1989, 35, 329;
35. C. Stockheim, K. Wieghardt, B. Nuber, J. Weiss, U. Flörke and H.-J. Haupt, J. Chem. Soc., Dalton Trans., 1991, 1487;
36. P. Knopp, K. Wieghardt, B. Nuber and J. Weiss, Z. Naturforsch., Teil B, 1991, 46, 1077;
37. A. Bodner, P. Jeske, T. Weyhermüller, K. Wieghardt, E. Dubler, H. Schmalle and B. Nuber, Inorg. Chem., 1992, 31, 3737;
38. P. Jeske, G. Haselhorst, T. Weyhermuller, K. Wieghardt and B. Nuber, Inorg. Chem., 1994, 33, 2462;
39. G. C. Silver and W. C. Trogler, J. Am. Chem. Soc., 1995, 177, 3983;
40. G. C. Silver, P. Gantzel and W. C. Trogler, Inorg. Chem., 1995, 34, 2487;
41. S.-M. Yang, W.-C. Cheng, S.-M. Peng, K.-K. Cheung and C.-M. Che, J. Chem. Soc., Dalton Trans., 1995, 2955 and refs. therein.
42. F. H. Allen, J. E. Davies, J. J. Galloy, O. Johnson, O. Kennard, C. F. Macrae, E. M. Mitchell, G. F. Mitchell, J. M. Smith and D. G. Watson, J. Chem. Inf. Comput. Sci., 1991, 31, 187.
43. Quanta/CHARMm, version 22.2, Molecular Simulations Inc., Burlington, MA, 1995.
44. P. J. A. Ribeiro-Claro, A. M. Amado, M. P. M. Marques and J. J. C. Teixeira-Dias, J. Chem. Soc., Perkin Trans., 2, 1996, 1161.