A simple method with liquid chromatography/tandem mass spectrometry for the determination of the six trichothecene mycotoxins in rice medium

Bioscience, Biotechnology and Biochemistry

Volumn 70, Issue 1, 2006, Pages 230-236

  Sagawa, Norifumi ^a   Takino, Takashi ^a   Kurogochi, Shin ^a  

^a BAYER AG   (Germany)

Author keywords

Deoxynivalenol; Ergosterol; LC MS MS; Matrix effect; Trichothecene mycotoxin

Indexed keywords

ACETONITRILE; BIOMASS; BIOSYNTHESIS; CROPS; IONIZATION; MASS SPECTROMETRY;

DEOXYNIVALENOL; ERGOSTEROL; LC-MS/MS; MATRIX EFFECT; TRICHOTHECENE MYCOTOXIN;

LIQUID CHROMATOGRAPHY;

MYCOTOXIN; TRICHOTHECENE DERIVATIVE;

ARTICLE; CALIBRATION; CELL PROLIFERATION; CHEMICAL STRUCTURE; CHEMISTRY; CULTURE MEDIUM; CYTOLOGY; FUSARIUM; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METHODOLOGY; RICE;

CALIBRATION; CELL PROLIFERATION; CHROMATOGRAPHY, LIQUID; CULTURE MEDIA; FUSARIUM; MASS SPECTROMETRY; MOLECULAR STRUCTURE; MYCOTOXINS; ORYZA SATIVA; TRICHOTHECENES;

ACETONITRILE; BIOMASS; BIOSYNTHESIS; IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETERS; RICE;

FUNGI; GIBBERELLA ZEAE; HUMAN ECHOVIRUS 1;

EID: 31444440382     PISSN: 09168451     EISSN: 13476947     Source Type: Journal    
DOI: 10.1271/bbb.70.230     Document Type: Article

References (14)

1. Pitt, J. I., Toxigenic fungi and mycotoxins. Br. Med. Bull., 56, 184-192 (2000).
2. Placinta, C. M., D'Mello, J. P. F., and Macdonald, A. M. C., A review of worldwide contamination of cereal grains and animal feed with Fusarium mycotoxins. Anim. Feed Sci. Tech., 78, 21-37 (1999).
3. D'Mello, J. P. F., Placinta, C. M., and Macdonald, A. M. C., Fusarium mycotoxins: a review of global implications for animal health, welfare and productivity. Anim. Feed Sci. Tech., 80, 183-205 (1999).
4. Langseth, W., and Rundberget, T., Instrumental methods for determination of nonmacrocyclic trichothecenes in cereals, foodstuffs and cultures. J. Chromatogr. A, 815, 103-121 (1998).
5. Sugita-Konishi, Y., and Kumagai, S., Toxicity of mycotoxins related with head blight diseases in wheat and establishment of provisional standard for tolerable level of DON in wheat. Mycotoxins (in Japanese), 55, 49-53 (2005).
6. Yoshizawa, T., and Morooka, N., Comparative studies on microbial and chemical modifications of trichothecene mycotoxins. Appl. Microbiol., 30, 38-43 (1975).
7. Yoshizawa, T., and Morooka, N., Biological modification of trichothecene mycotoxins: acetylation and deacetylation of deoxynivalenols by Fusarium spp. Appl. Microbiol., 29, 54-58 (1975).
8. Greenhalgh, R., Levandier, D., Adams, W., Miller, J., Blackwell, B., McAlees, A., and Taylor, A., Production and characterization of deoxynivalenol and other secondary metabolites of Fusarium culmorum (CMI 14764, HLX 1503). J. Agric. Food Chem., 34, 98-102 (1986).
9. Witt, M., Hart, L., and Pestka, J., Purification of deoxynivalenol (vomitoxin) by water-saturated silica gel chromatography. J. Agric. Food Chem., 33, 745-748 (1985).
10. Langseth, W., Ghebremeskel, M., Kosiak, B., Kolsaker, P., and Miller, D., Production of culmorin compounds and other secondary metabolites by Fusarium culmorum and F. graminearum strains isolated from Norwegian cereals. Mycopathologia, 152, 23-34 (2000).
11. Lagana, A., Curini, R., D'Ascenzo, G., Leva, I., Faberi, A., and Pestorini, E., Liquid chromatography/tandem mass spectrometry for the identification and determination of trichothecenes in maize. Rapid Commun. Mass Spectrom., 17, 1037-1043 (2003).
12. Cavaliere, C., Foglia, P., Pastorini, E., Samperi, R., and Lagana, A., Development of a multiresidue method for analysis of major Fusarium mycotoxins in corn meal using liquid chromatography/tandem mass spectrometry. Rapid Commun. Mass Spectrom., 19, 2085-2093 (2005).
13. Suga, K., Mochizuki, N., Harayama, K., and Yamashita, H., Analysis of trichothecenes in barley tea and beer by liquid chromatography/tandem mass spectrometry. Shokuhin Eiseigaku Zasshi (in Japanese), 45, 307-312 (2004).
14. Schwadorf, K., and Muller, H., Determination of ergosterol in cereals, mixed feed components, and mixed feeds by liquid chromatography. J. AOAC Int., 72, 457-462 (1989).