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3142745201
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+ - 8CO).
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3142679351
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note
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w = 0.1283. The structure was solved by direct methods and expanded by Fourier techniques. The final refinements were accomplished by the full-matrix least-squares method with anisotropic thermal parameters for non-hydrogen atoms. Hydrogen atoms were included but not refined. The calculations were performed using the SHELXTL-97 program.
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