Stability of fat-soluble and water-soluble vitamins in artificially prepared, vitamin-enriched, lyophilized serum

Journal of Clinical Laboratory Analysis

Volumn 18, Issue 4, 2004, Pages 240-246

  Ihara, Hiroshi ^a   Hashizume, Naotaka ^a   Matsubayashi, Tadashi ^b   Futaki, Koichi ^b   Yoshida, Masayuki ^c   Sagawa, Naotoshi ^d   Fujisaki, Makoto ^d   Mita, Kazuo ^e   Kadota, Akira ^f  

^a TOHO UNIVERSITY OHASHI MEDICAL CENTER   (Japan)

^b Inovation Research Center   (Japan)

^c Roche Diagnostics KK   (Japan)

^d Mitsubishi Kagaku Bio Clinical Laboratories Inc   (Japan)

^e TSL   (Japan)

^f Kyowa Medex Co Ltd   (Japan)

Author keywords

Lyophilized serum; Reference value; Standard reference materials 968c (SRM 968c); Vitamins

Indexed keywords

ALPHA TOCOPHEROL; ASCORBIC ACID; CHOLESTEROL; CYANOCOBALAMIN; FOLIC ACID; RETINOL; THIAMINE; VITAMIN;

ARTICLE; CONTROLLED STUDY; DILUTION; DRUG STABILITY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HUMAN TISSUE; LYOPHILISATE; REFERENCE VALUE; RELATIVE DENSITY; SERUM; STATISTICAL ANALYSIS; STORAGE TEMPERATURE; VISCOSITY; VOLUNTEER;

ASCORBIC ACID; CHOLESTEROL; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CRYOPRESERVATION; DRUG STABILITY; FOLIC ACID; FREEZE DRYING; HUMANS; REFERENCE VALUES; THIAMINE; VITAMIN A; VITAMIN B 12; VITAMIN E; VITAMINS;

EID: 3142579749     PISSN: 08878013     EISSN: None     Source Type: Journal    
DOI: 10.1002/jcla.20030     Document Type: Article

References (19)

1. National Research Council. Recommended dietary allowances, 11th ed. Washington, DC: National Academy Press; 1998. p 1-16.
2. The Study Circle for Health and Nutrition Information. Recommended dietary allowances for the Japanese, 6th rev. Dietary reference intakes (Jpn). Tokyo: Daiich-Shuppan Publishing Co., Ltd.; 1999. p 81-127.
3. McCormick DB, Greene HL, Fairbanks VF, Klee GG. Vitamins, vitamin B12, and folic acid. In: Burtis CA, Ashwood ER, editors. Tiets textbook of clinical chemistry, 2nd ed. Philadelphia: WB Saunders Company; 1994. p 1275-1316, p 2046-2057.
4. Turley CP, Brewster MA. Vitamin A and vitamin E. In: Pesce AJ, Kaplan LA, editors. Methods in clinical chemistry. St. Louis: The CV Mosby Company; 1987. p 551-590.
5. Ito S, Kudo S, Mita K. Determination of vitamin A (Jpn). Rinsho Kensa 2001;45:1077-1082.
6. Japan Committee for Vitamin Laboratory Standards. Proposed standard for human blood vitamin B1 value using HPLC. Biofactors 1999;10:295-299.
7. Katsumata M. Studies on thiamine. (II) On the thiochrome production by mercuric salts (Jpn). Seikagaku 1956;28:368-371.
8. Japan Committee for Vitamin Laboratory Standards. Proposed standard for total ascorbic acid values in human plasma: HPLC procedure as a reference method (Jpn). J Jpn Soc Nutr Food Sci 2001;54:41-44.
9. Ihara H, Hashizume N, Hirano A, Okada M. Determination of vitamin C (Jpn). Rinsho Kensa 2001;45:1104-1111.
10. Ihara H, Ishigaki H, Shino Y, et al. Clinical and analytical evaluation of the simultaneous HPLC assay of retinol and α-tocopherol. J Nutr Sci Vitaminol 2000;46:257-262.
11. Catignani GL, Bieri JG. Simultaneous determination of retinol and α-tocopherol in serum or plasma by liquid chromatography. Clin Chem 1983;29:708-712.
12. Penttinen HK. Differences in thiochrome fluorescence produced by thiamine and its mono-, di-, and triphosphate esters. Acta Chem Scand 1976;30:659-663.
13. Eitenmiller RR, Landen WO. Vitamin analysis for the health and food sciences. Baca Raton: CRC Press; 1998. p 3-148, p 223-270.
14. Scientific Division of Japan Society of Clinical Chemistry. Proposed standard for certified enzyme reference materials (ERM). Jpn J Clin Chem 2000;29:77-92.
15. National Committee for Clinical Laboratory Standards. Preparation and validation of commutable frozen human serum pools as secondary reference materials for cholesterol measurement procedures; Approved guideline. Myers GL, Eckfeldt JH, Greenberg N, Levine JB, Miller WG, Wiebe DA, eds. Wayne, PA: NCCLS. p 1-25. 1999;19:C37-A.
16. Thomas JB, Duewer DL, Kline MC, Sharpless KE. The stability of retinol, α-tocopherol, trans-lycopene, and trans-β-carotene in liquid-frozen and lyophilized serum. Clin Chim Acta 1998;276: 75-87.
17. Jordan P, Brubacher D, Moser U, Stahelin HB, Gey KF. Vitamin E and vitamin A concentrations in plasma adjusted for cholesterol and triglycerides by multiple regression. Clin Chem 1995;41: 924-927.
18. Dhariwal KR, Hartzell WO, Levine M. Ascorbic acid and dehydroascorbic acid measurements in human plasma and serum. Am J Clin Nutr 1991;54:712-716.
19. Thame G, Guerra-Shinohara EM, Moron AF. Serum folate by two methods in pregnant women carrying fetuses with neural tube defects. Clin Chem 2002;48:1094-1095.