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Volumn 44, Issue 20, 1988, Pages 6337-6344

A short route to dehydro [12] annulenes.

(2) Huynh, Chanh a Linstrumelle, Gerard a

a ECOLE NORMALE SUPÉRIEURE (France)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 3142525222 PISSN: 00404020 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4020(01)89821-5 Document Type: Article

Times cited : (118)

References (22)

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11
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- Under the same conditions, by using an unencumbered amine such as piperidine, 1 and 2 wereobtained in 56 % and 31 % respectively ; however, by using 3 equiv. (instead of 1.5 equiv.) of 2-methyl-3-butyn-2-ol, the diol 2 was obtained in 82 % yield.

12
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- Under Pd-Cu conditions, when the reaction was performed at 22 % for 24h in triethylamine, piperidine or propylamine, by using 2-methyl-3-butyn-2-ol in excess (3 equiv.), the monosubstituted product 1 was obtained in 25% yield. The disubstituted product 2 was not formed.

13
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- The step wise reaction of 1,2-dibromobenzene with acetylenes has been recently reported :
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- 16

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18
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21
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- 3) : d = 87.16; 92.06; 96.04; 112.19; 125.17; 125.64; 128.10; 128.38; 128.58; 132.11; 132.34ppm.

22
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- Vavshavskii¹ Kiseleva²

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.