Nickel(II) and copper(II) complexes with triethylenetetraaminehexaacetic acid: From binuclear complex to 1D coordination polymer

Inorganic Chemistry Communications

Volumn 9, Issue 2, 2006, Pages 192-195

  Shi, Wei ^a   Dai, Yan ^a   Zhao, Bin ^a   Song, Hai Bin ^a   Wang, Hong Gen ^a   Cheng, Peng ^a  

^a NANKAI UNIVERSITY   (China)

Author keywords

Copper(II) complex; Crystal structure; Nickel(II) complex; Triethylenetetraaminehexaacetic acid

Indexed keywords

EID: 31344482313     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2005.11.002     Document Type: Article

References (24)

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19. 2 = 0.0896 [I > 2σ(I)]. Structural measurements of all complexes were performed on a computer controlled Bruker SMART 1000 CCD diffractometer equipped with graphite-monochromated Mo Kα radiation with radiation wavelength 0.71073 Å by using the ω-φ scan technique. The structures were solved by direct methods and refined with the full-matrix least-squares technique using the SHELXS-97 and SHELXL-97 programs [11]. CCDC Nos. 280726 (1) and 177964 (2) contain the supplementary crystallographic data. These data can be obtained via the Cambridge Crystallographic Data Centre deposit@ccdc.cam.ac.uk http://www.ccdc.cam.ac.uk/deposit.
20. 24: found: C, 24.04; H, 5.26; N, 6.25. Calc.: C, 24.15; H, 5.40; N, 6.26.
21. G.M. Sheldrick SHELXS-97, Program for X-ray Crystal Structure Solution 1997 Göttingen University Germany
22. G.M. Sheldrick SHELXL-97, Program for X-ray Crystal Structure Refinement 1997 Göttingen University Germany
23. 2O was reported in the literature [7a], except that the number of lattice water molecules is different.
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