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2) = 0.975. Hydrogen atoms were included in structure factor calculations at idealized positions and were allowed to ride on attached carbon atoms with relative isotropic displacement coefficients. All non-hydrogen atoms, except carbon atoms of phenyl groups, were refined anisotropically.
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0004150157
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Measurements were performed by Dr. Richard Noll (Manager, SEM Facility at Materials Center-Instrumentations, University of Wisconsin - Madison) on a LEO DMS 1530 field emission scanning electron microscope (JEOL JSM-6100).
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2O with a MeCN solution of 1, were identified as 1 via IR amd X-ray crystallographic analysis (approximate yield, 10-15%). This much simpler, direct preparative route is preferable to the original one (ref 5), and optimization of the reaction boundary conditions should give rise to a higher yield of 1.
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