Measurement of magnetic susceptibility and calculation of shape factor of NMR samples

Journal of Magnetic Resonance

Volumn 178, Issue 2, 2006, Pages 237-247

  Hoffman, Roy E ^a  

^a HEBREW UNIVERSITY OF JERUSALEM   (Israel)

Author keywords

BMS shift; Chemical shift; Shape factor; Susceptibility

Indexed keywords

CHEMICAL ANALYSIS; MAGNETIC SUSCEPTIBILITY; SOLVENTS; TEMPERATURE MEASUREMENT;

BMS SHIFT; CHEMICAL SHIFT; SHAPE FACTOR; SUSCEPTIBILITY;

NUCLEAR MAGNETIC RESONANCE;

EID: 30844440723     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2005.09.009     Document Type: Article

References (37)

1. S.C.-K. Chu, Y. Xu, J.A. Balschi, and C.S. Springer Jr. Bulk magnetic susceptibility shifts in NMR studies of compartmentalized samples: use of paramagnetic reagents Magn. Reson. Med. 13 1990 239 262
2. C.J. Durrant, M.P. Hertzberg, and P.W. Kuchel Magnetic susceptibility: further insights into macroscopic and microscopic fields and the sphere of Lorentz Conc. Magn. Reson. A 18 2003 72 95
3. D.J. Philp, W.A. Bubb, and P.W. Kuchel Chemical shift and magnetic susceptibility contributions to the separation of intracellular and supernatant resonances in variable angle spinning NMR spectra of erythrocyte suspensions Magn. Reson. Med. 51 2004 441 444
4. Commission on Molecular Structure and Spectroscopy, Recommendations for the presentation of NMR data for publications in chemical journals, Pure Appl. Chem. 29 (1972) 627-628.
5. F.H.A. Rummens, and R.H. Krystynhak Intermolecular interaction in nuclear magnetic resonance. VII. The role of the internal reference in aromatic solvent induced shifts J. Am. Chem. Soc. 94 1972 6914 6921
6. M.R. Bacon, and G.E. Maciel Solvent effects of the five shielding constants in tetramethylsilane and cyclohexane J. Am. Chem. Soc. 95 1973 2413 2426
7. R.E. Hoffman Variations on the chemical shift of TMS J. Magn. Reson. 163 2003 325 331
8. 1H chemical shift of tetramethylsilane in chloroform, methanol and dimethylsulfoxide J. Magn. Reson. 176 2005 87 98
9. A. DeMarco pH dependences of internal references J. Magn. Reson. 26 1977 527 528
10. R.K. Harris, E.D. Becker, S.M. Cabral de Menezes, R. Goodfellow, and P. Granger NMR nomenclature: nuclear spin properties and conventions for chemical shifts. IUPAC recommendations 2001 Pure Appl. Chem. 73 2001 1795 1818
11. D.S. Wishart, B.D. Sykes, and F.M. Richards Relationship between nuclear magnetic resonance chemical shift and protein secondary structure J. Mol. Biol. 222 1991 311 333
12. D.S. Wishart, B.D. Sykes, and F.M. Richards The chemical shift index: a fast and simple method for the assignment of protein secondary structure through NMR spectroscopy Biochemistry 31 1992 1647 1651
13. L. Poulad-Meyer, Extraction studies of the transfer of acidic or basic compounds from aqueous phases into multicomponent organic extracting media, Thesis Hebrew University of Jerusalem, 2001.
14. Y.-F. Lam, and G. Kotowycz Caution concerning the use of sodium 2,2-dimethyl-2-silapentane-5-sulfonate (DSS) as a reference for protein NMR chemical shift studies FEBS Lett. 78 1977 181 183
15. 15N chemical shift referencing in biomolecular NMR J. Biomol. NMR. 6 1995 135 140
16. R.K. Harris, E.D. Becker, S.M. Cabral de Menzes, P. Granger, R.E. Hoffman, K. Zilm, NMR chemical shifts: updated conventions, IUPAC Project 2003-006-1-100. Available from: 〈www.iupac.org〉.
17. R.C. Weast, M.J. Astle (Eds.), Handbook of Chemistry and Physics, 62nd edition. CRC Press, Boca Raton, FL, 1982.
18. Landolt-Börnstein Zahlenwerte und Funktionen aus Physik Chemie Astronomie Geophysik und Technik, 6th edition, 2 Band, 10 Teil, in: W.R. Angus, J. Favède, J. Hoarau, A. Pacault (Eds.), Magnetic Properties II, Springer-Verlag, Berlin, 1967.
19. F.D. Doty, G. Entzminger, and Y.A. Yang Magnetism in high-resolution NMR probe design. I: General methods Conc. Magn. Reson. 10 1998 133 156
20. E.D. Becker High Resolution NMR 2000 Academic Press San Diego, CA p. 91
21. J.D. Jackson Classical Electrodynamics second ed. 1975 Wiley New York
22. D. Craik Magnetism: Principles and Applications 1995 Wiley New York pp. 418-420
23. 129Xe NMR as a probe for blood oxygenation Magn. Reson. Med. 43 2000 491 496
24. L. Li Magnetic susceptibility quantification for arbitrarily shaped objects in inhomogeneous fields Magn. Reson. Med. 46 2001 907 916
25. L. N. Mulay, in: A. Weissberger, B.W. Rossiter (Eds.), Techniques of Chemistry, Wiley-Interscience, New York, vol. 4, 1972, 431.
26. R. Engel, D. Halpern, and S. Bienenfeld Determination of magnetic moments in solution by nuclear magnetic resonance spectrometry Anal. Chem. 45 1973 367 369
27. J.R. Zimmerman, and M.R. Foster Standardization of N.M.R. high resolution spectra J. Phys. Chem. 61 1957 282 289
28. P.W. Kuchel, B.E. Chapman, W.A. Bubb, P.E. Hansen, C.J. Durrant, and M.P. Hertzberg Magnetic susceptibility: solutions, emulsions and cells Conc. Magn. Reson. A 18 2003 56 71
29. A.N. Garroway Magic-angle sample spinning of liquids J. Magn. Reson. 1982 168 171
30. 1H MAS NMR spectra of cell suspensions Magn. Reson. Med. 50 2003 515 521
31. S.E. Ashbrook, and S. Wimperis SCAM-STMAS: satellite-transition MAS NMR of quadrupolar nuclei with self-compensation for magic-angle misset J. Magn. Reson. 162 2003 402 416
32. S.E. Ashbrook, and S. Wimperis High-resolution NMR spectroscopy of quadrupolar nuclei in solids: satellite-transition MAS with self-comensation for magic-angle misset J. Am. Chem. Soc. 124 2002 11602 11603
33. K. Frei, and H.J. Bernstein Method for determining magnetic susceptibilities by NMR J. Chem. Phys. 37 1962 1891 1892
34. P. Granger, M. Piotto, O. Assémat, M. Bourdonneau, NMR chemical shift measurements revisited: high precision measurements, Conc. Magn. Reson. (submitted).
35. "Physical and Thermodynamic Properties of Pure Chemicals." American Institute of Chemical Engineers, Design Institute for Physical Properties, 1998-2004. See www.aiche.org for availability on-line and in printed form.
36. Aldrich catalog 2005.
37. 13C: application to polycyclic aromatic hydrocarbon anions Magn. Reson. Chem. 39 2001 489 494