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6-SP-X complex. Formation of the A ring adducts, their photochromism (half-life of the colored species ≤ 10 min), and diastereoisomerism including exclusive formation of one of the two diastereomers upon UV irradiation were reported: Miyashita, A.; Iwamoto, A.; Kuwayama, T.; Shitara, H.; Aoki, Y.; Hirano, M.; Nohira, H. Chem. Lett. 1997, 965.
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27
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30344451583
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note
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1H NMR spectra. The LH NMR suggested formation of a mixture of isomers, which could not be separated.
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28
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0003686701
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Springer: Berlin
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Pretsch, P. D.; Seible, J.; Simon, W.; Clerc, T. Strukturaufklälung organischer Verbindungen, 2nd ed.; Springer: Berlin, 1981.
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(a) Godsi, O.; Peskin, U.; Kapon, M.; Natan, E.; Eichen, Y. Chem. Commun. 2001, 2132.
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(b) Raymo, F. M.; Giordani, S.; White, A. J. P.; Williams, D. J. J. Org. Chem. 2003, 68, 4158.
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31
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30344438442
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note
-
-1, current R1 = 0.1160 for 1016 reflections with I > 2σ(I), wR2 = 0.3008 for all observed 2887 reflections with 174 parameters (isotropic refinements for all non-hydrogen atoms; H atoms not included in the refinement).
-
-
-
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32
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30344439405
-
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note
-
-1, current R1 = 0.104 for 3213 reflections with I > 2σ(I), wR2′= 0.303 for all observed 3620 reflections with 240 parameters.
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33
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30344449365
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The open forms of free SP-X molecules were also characterized by X-ray crystallography.7
-
The open forms of free SP-X molecules were also characterized by X-ray crystallography.7
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34
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10744226746
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1a: Raic-Malic, S.; Tomaskovic, L.; Mrvos-Sermek, D.; Prugovecki, B.; Cetina, M.; Grdisa, M.; Pavelic, K.; Mannschreck, A.; Balzarini, J.; De Clercq, E.; Mintas, M. Bioorg. Med. Chem. 2004, 12, 1037.
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Raic-Malic, S.1
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Cetina, M.5
Grdisa, M.6
Pavelic, K.7
Mannschreck, A.8
Balzarini, J.9
De Clercq, E.10
Mintas, M.11
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35
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0038433859
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1c: Karaev, K. Sh.; Furmanova, N. G.; Belov, N. V. Proc. Natl. Acad. Sci. USSR 1982, 262, 877.
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Karaev, K.Sh.1
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Belov, N.V.3
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36
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0000634537
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Clegg, W.; Norman, N. C.; Flood, T.; Sallans, L.; Kwak, W. S.; Kwiatkowski, P. L.; Lasch, J. G. Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1991, 47, 817.
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Clegg, W.1
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Kwak, W.S.5
Kwiatkowski, P.L.6
Lasch, J.G.7
-
37
-
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30344475107
-
-
The open form S was not converted to the closed form 4 under thermal reaction conditions but upon UV irradiation (see below)
-
The open form S was not converted to the closed form 4 under thermal reaction conditions but upon UV irradiation (see below).
-
-
-
-
38
-
-
30344435181
-
-
note
-
1/2 = 0.28 V)) attributed to the open form 5/5′c. Switching of the electrochemical properties is evident from the charts, but the assignments of the redox processes of 4c and 5/5′c could not be made
-
-
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39
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0031589096
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(b) Gusev, O. V.; Ievlev, M. A.; Peterleitner, M. G.; Pregudova, S. M.; Denisovich, L. I.; Petrovskii, P. V.; Ustynyuk, N. A. J. Organomet. Chem. 1997, 534, 57.
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Petrovskii, P.V.6
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40
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0028804716
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Torres, S.1
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46
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0003567345
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The DIRDIF program system
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University of Nijmegen, Nijmegen, The Netherlands
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Beurskens, P. T.; Admiraal, G.; Beurskens, G.; Bosman, W. P.; Garcia-Granda, S.; Gould, R. O.; Smits, J. M. M.; Smykalla, C. The DIRDIF Program System, Technical Report of the Crystallography Laboratory; University of Nijmegen, Nijmegen, The Netherlands, 1992.
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Technical Report of the Crystallography Laboratory
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Beurskens, P.T.1
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Smits, J.M.M.7
Smykalla, C.8
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