Carbamates from alcohol diversity: A simple solution phase library method

Tetrahedron Letters

Volumn 47, Issue 6, 2006, Pages 967-968

  Hamilton, Gregory L ^a   Backes, Bradley J ^a  

^a ABBOTT LABORATORIES   (United States)

Author keywords

Carbamates; Library synthesis; Parallel synthesis

Indexed keywords

ALCOHOL; CARBAMIC ACID; RESIN;

ARTICLE; CHEMICAL COMPOSITION; CHEMICAL REACTION; CHEMICAL STRUCTURE; LIQUID CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; SYNTHESIS;

EID: 30344459719     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2005.11.139     Document Type: Article

References (6)

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4. A.K. Ghosh, T.T. Duong, S.P. McKee, and W.J. Thompson Tetrahedron Lett. 20 1992 2781 2784
5. Yields for this one-pot process were comparable to those obtained using the serial method in which an extractive purification of the mixed carbonate was employed, followed by amine addition.
6. 3CN was added. The reaction was stirred for 3 h, concentrated and purified over silica gel to provide the products in analytically pure form.