Multidimensional gas chromatography-olfactometry for identification and prioritization of malodors from confined animal feeding operations

ASAE Annual International Meeting 2004

Volumn , Issue , 2004, Pages 5531-5545

  Wright, Donald W ^a   Eaton, David K ^a   Nielsen, Lawrence T ^a   Kuhrt, Fred W ^a   Koziel, Jacek A ^b   Spinhirne, Jarett P ^b   Parker, David B ^c  

^a Microanalytics a MOCON Company   (United States)

^b TEXAS A AND M UNIVERSITY   (United States)

^c WEST TEXAS A AND M UNIVERSITY   (United States)

Author keywords

Agricultural odor analysis; Farm odor; GC O; GC Olfactometry; Livestock housing; Malodor analysis; Multidimensional gas chromatography; Para cresol; Solid phase microextraction; SPME; Volatile organic compounds

Indexed keywords

AGRICULTURAL ODOR ANALYSIS; FARM ODOR; GC-O; GC-OLFACTOMETRY; LIVESTOCK HOUSING; MALODOR ANALYSIS; MULTIDIMENSIONAL GAS CHROMATOGRAPHY; PARA-CRESOL; SOLID PHASE MICROEXTRACTION; SPME;

AGRICULTURE; CONSUMER PRODUCTS; EXTRACTION; FARMS; GAS CHROMATOGRAPHY; VOLATILE ORGANIC COMPOUNDS;

ODOR CONTROL;

ANIMALS; EXTRACTION; GAS CHROMATOGRAPHY; ODOR CONTROL; VOC;

EID: 30044448306     PISSN: None     EISSN: None     Source Type: Conference Proceeding    
DOI: None     Document Type: Conference Paper

References (19)

1. Chai, M. and J. Pawliszyn. 1995. Analysis of environmental air samples by solid phase microextraction and gas chromatography / ion trap mass spectrometry. Environ. Sci.& Technol. 29(3): 693-701.
2. Chai, M. and Y. Tang. 1997: Solid phase microextraction (SPME) analysis of whole air samples. Intern. Environ. Anal. Chem., 72(1): 77-82.
3. Devos, M., F. Patte, J. Roualt, P. Laffort, and L.J. Van Gemert. 1990. Standardized Human Olfactory Thresholds. IRL Press at Oxford Press, NY, New York.
4. Gordon, B.M.; Uhrig, M.S.; Borgerding, M.F.; Chung, H.L.; Coleman, W.M.; Elder, J.F.; Giles, J.A.; Moore, D.S.; Rix, C.E. and White, E. L. 1988. Analysis of flue-cured tobacco essential oil by hyphenated analytical techniques. J. Chrom. Sci. 26(April): 174-180.
5. Hutchinson, G.L., A.R. Mosier, and C.E. Andre. 1982. Ammonia and amine emissions from a large cattle feedlot. J Environ. Qual. 11(2): 288-293.
6. Keener, K.M., J. Zhang, R.D. Bottcher, and R.D. Munilla. 2002. Evaluation of thermal desorption for the measurement of artificial swine odorants in the vapor phase. Trans. ASAE 45(5): 1579-1584.
7. McGinn, S.M., H.H Jantzen and T. Coates. 2003. Atmospheric ammonia, volatile fatty acids and other odorants near beef feedlots. J Environ. Qual. 32: 1173-1182.
8. Mosier, A.R., C.E. Andre and F.G. Jr Viets. 1973. Identification of aliphatic amines volatilized from cattle feedyard. Environ. Sci. & Technol. 7(7): 642-644.
9. MSDS. 2002. CAS number 7783-06-4. Aldrich Chemical Company, Inc., Milwaukee, Wi., USA. Valid period 11/2001 to 01/2002.
10. Nielsen, L.T., D.K. Eaton and D.W. Wright. 2001. High flavor impact components: the case of beta-demascenone and 2′-aminoacetophenone. In Proceedings of American Society of Brewing Chemists Conference, Victoria, BC, Canada.
11. Nielsen, L.T., D.K. Eaton, D.W. Wright and B. French. 2001. Beer, taco shells and Mexican free-tailed bats. In Proceedings of American Chemical Society - Southwest Regional Conference.
12. Nielsen, L.T., D.K. Eaton, D.W. Wright and B. French. 2004. Identification of characteristic odors of Mexican free-tailed bat roosts by gas chromatography - olfactometry. Presubmission manuscript in development - personal communication between investigators.
13. Oehrl, L.L., K.M. Keener, R.D. Bottcher, R.D. Munilla, and K.M. Connely. 2001. Characterization of odor components from swine housing dust using gas chromatography. Applied Eng. in Agric. 17(5): 659-661.
14. Pawliszyn J. Solid Phase Microextraction - Theory and Practice; Wiley-VCH: New York, 1997.
15. Spinhirne, J.P., J.A. Koziel, D.B. Parker, D. Williams, N.A. Cole, J.M. Sweeten. 2002. Screening for volatile organic fatty acids in agricultural air using solid-phase microextraction and GC-MS. Paper #024163 In Proceedings of the 2002 ASAE/CIGR Annual Intl Meeting, Chicago, IL, 2002.
16. USEPA Website. 2003. Odor characterization, assessment and sampling. In: Guide to Field Storage of Biosolids - Appendix A. Available at www.epa.gov, accessed July 1, 2003.
17. rd International ASAE Conference on Air Pollution from Agriculture, Research Triangle Park, NC, October 2003.
18. Wright, D.W., K.O. Mahlerand L/B. Ballard. 1986. The application of an expanded multidimensional GC system to complex fragrance evaluations. J Chrom. Sci. 24(60): 60-65.
19. Wright, D.W. 1997. Application of multidimensional gas chromatography techniques to aroma analysis. In: Techniques for Analyzing Food Aroma (Ray Marsili, ed.). Marcel Dekker, Inc., NY, 113-141.