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29544451216
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note
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2: 324.1429; found: 324.1426.
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16
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29544431728
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note
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For the percent extraction (%Ex), a water-saturated chloroform solution of ligand (5.00 ml, 1.00 mM) and an aqueous solution of metal picrate (5.00 ml, 1.00 mM) were placed in a stop-cocked flask, and the flask was shaken in a thermostated water bath for 2 h at 25 ± 0.2°C. The concentration of metal picrate in aqueous phase was determined at 354 nm. Mercury(II) picrate was excluded due to its free extraction.
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17
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29544450010
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note
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+); m.p. 197-199°C.
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18
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29544434303
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note
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2 = 0.1463) for 6812 independent reflections [I > 2σ(I)].
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20
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37049084846
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