Preparative counter-current chromatography isolation of liensinine and its analogues from embryo of the seed of Nelumbo nucifera GAERTN. Using upright coil planet centrifuge with four multilayer coils connected in series

Journal of Chromatography A

Volumn 1041, Issue 1-2, 2004, Pages 153-162

  Wu, Shihua ^a,b   Sun, Cuirong ^a   Cao, Xiaoji ^a   Zhou, Hui ^a   Zhang, Hong ^a,c   Pan, Yuanjiang ^a  

^a ZHEJIANG UNIVERSITY   (China)

^b ZHEJIANG UNIVERSITY   (China)

^c ZHEJIANG GONGSHANG UNIVERSITY   (China)

Author keywords

Alkaloids; Counter current chromatography; Isoliensinine; Liensinine; Neferine; Nelumbo nucifera; Pharmaceutical analysis; Plant materials; Preparative chromatography

Indexed keywords

MOLECULAR STRUCTURE; ORGANIC SOLVENTS; SEED; SOILS;

ELECTROSPRAY IONIZATION; MULTILAYER COILS;

CHROMATOGRAPHIC ANALYSIS;

ACETIC ACID ETHYL ESTER; ALKALOID; CARBON TETRACHLORIDE; CHLOROFORM; HERBACEOUS AGENT; ISOLIENSININE; LIENSININE; METHANOL; NEFERINE; PETROLEUM; SOLVENT; UNCLASSIFIED DRUG; WATER;

ARTICLE; CENTRIFUGE; COUNTER CURRENT CHROMATOGRAPHY; DRUG ISOLATION; DRUG PURIFICATION; DRUG PURITY; DRUG STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; NELUMBO; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHASE SEPARATION; PRIORITY JOURNAL;

COUNTERCURRENT DISTRIBUTION; ISOQUINOLINES; MOLECULAR STRUCTURE; NELUMBO; PHENOLS; SEEDS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

NELUMBO; NELUMBO NUCIFERA;

EID: 2942620337     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2004.05.003     Document Type: Article

References (18)

1. Ni Z. Acta. Hortic. Sinica. 10:1983;207
2. Q.V. Nguyen, Exporting Lotus to Asia-An Agronomic and Physiological Study. Rural Industries Research and Development Corporation (RIRDC). NSW Agriculture, Horticultural Research and Advisory Station, Gosford, Australia, 2001.
3. Liu Y., Sun B. J. Changjiang Vegetables. 4:2003;5
4. Chao T., Chou Y., Young P., Chou T. Sci. Sinica. 11:1962;215
5. Tomita M., Furukawa H., Yang T.H., Lin T.J. Tetrahedron Lett. 37:1964;2637
6. Kametani T., Nemoto H., Kobari T., Takano S. J. Heterocyclic Chem. 7:1970;181
7. Guo M., Chen L. Zhongcaoyao. 15:1984;3
8. Nishibe S., Tsukamoto H., Kinoshita H., Kitagawa S., Sakushima A. J. Nat. Prod. 49:1986;548
9. Wang J., Hu X., Yin W., Cai H. Zhongguo Zhongyao Zazhi. 16:1991;673
10. Xu L., Yao C., Chen J. Zhongcaoyao. 31:2000;956
11. Zhang H., Pan Y. J. Nanjing TCM Univ. (Nat. Sci.). 18:2002;382
12. Zhang X., Hu X., Luo S., Cai H., Yin W. Yaowu Fenxi Zazhi. 17:1997;110
13. Tanimura T., Pisano J.J., Ito Y., Bowman R.L. Science. 169:1970;54
14. Ito Y. J. Chromatogr. 538:1991;3
15. N.B. Mandava, Y. Ito (Eds.), Counter-current Chromatography: Theory and Practice, Marcel Dekker, New York, 1988.
16. Y. Ito, W.D. Conway (Eds.), High-Speed Countercurrent Chromatography, Wiley-Interscience: New York, 1996.
17. Wu S., Sun C., Wang K., Pan Y. J. Chromatogr. A. 1028:2004;171
18. Wu J., Ran H., Wang J., Sun H. Zhongcaoyao. 29:1998;362