Evaluation of boron doped diamond electrodes for organic electrosynthesis on a preparative scale

Journal of Applied Electrochemistry

Volumn 35, Issue 12, 2005, Pages 1265-1270

  Griesbach, Ulrich ^a   Zollinger, Daniel ^a,b   Pütter, Hermann ^a   Comninellis, Christos ^b  

^a BASF SE   (Germany)

^b EPFL   (Switzerland)

Author keywords

Biaryls; Boron doped diamond electrodes; Cleavage of C C bonds; Electrode stability; Oxime reduction

Indexed keywords

BORON; DIAMONDS; ELECTROCHEMISTRY; ELECTROLYTES; OXIDATION; SEMICONDUCTOR DOPING;

BORON DOPED DIAMOND ELECTRODES; CLEAVAGE OF C-C BONDS; ELECTRODE STABILITY; OXIME REDUCTION;

ELECTRODES;

EID: 29344454469     PISSN: 0021891X     EISSN: None     Source Type: Journal    
DOI: 10.1007/s10800-005-9038-2     Document Type: Article

References (23)

1. M. Fryda, Th. Mathée, S. Mulcahy, M. Höfer, L. Schäfer and I. Tröster, in 'The Electrochemical Society Interface, Spring 2003', (2003), pp. 40-44 and references cited therein.
2. P.-A. Michaud, E. Mahé, W. Haenni, A. Perret and Ch. Comninellis, Electrochem. Solid-St. 3 (2000) 77.
3. L.J.J. Janssen and M.H.A. Blijlevens, Electrochim. Acta 48 (2003) 3959.
4. M.S. Saha, T. Furuta and Y. Nishiki, Electrochem. Commun. 6 (2004) 201.
5. P.-A. Michaud, Ch. Comninellis, W. Haenni, A. Perret, J. Niesta, M. Fryda and L. Schaefer, in 'Electrochemical Society Proceedings', Vol. 2001-23 (2003), pp. 87-96.
6. European Patent EP 1 036 861 B1 (BASF AG).
7. German Patent DE 103 13 169 A1 (Degussa AG).
8. D. Zollinger, U. Griesbach, H. Pütter and Ch. Comninellis, Electrochem. Commun. 6 (2004) 600.
9. D. Zollinger, U. Griesbach, H. Pütter and Ch. Comninellis, Electrochem. Commun. 6 (2004) 605.
10. P. Canizares, M. Diaz, J.A. Dominguez, J. Garcia-Gomez and M.A. Rodrigo, Ind. Eng. Chem. Res. 41 (2002) 4187.
11. J. Iniesta, P.-A. Michaud, M. Panizza and Ch. Comninellis, Electrochem. Commun. 3 (2001) 346.
12. B. Marselli, J. Garcia-Gomez, P.-A. Michaud, M.A. Rodrigo and Ch. Comninellis, J. Electrochem. Soc. 150 (2003) D79.
13. D. Zollinger, Electrochemical Reactions at Diamond Electrodes in Aqueous and Non-aqueous Solutions Diploma (Swiss Federal Institute of Technology, Lausanne, 2004) Diploma thesis.
14. P. Loyson, S. Grouws and B. Zeelie, S. Afr. J. Chem. 55 (2002) 125 and references cited therein.
15. T. Shono, Y. Matsumura, K. Inoue and F. Iwasaki, J. Chem. Soc. Perkin Trans. I (1986) 73.
16. H.B. Martin, A. Argoita, U. Landau, A.B. Anderson and J.C. Angus, J. Electrochem. Soc. 143 (1996) L133.
17. 9 was prepared by Friedel-Crafts acylation of benzene with 4-chloro-butyryl chloride (W.J. Close, J. Am. Chem. Soc. 79 (1957) 1455) followed by oximation
18. (H.G.O. Becker, R. Beekert, G. Domschke, E. Fanghänel, W.D. Habicher, P. Metz, D.Pavel and K. Schwetlick, Organikum, Organisch-chemisches Grundpraktikum (Wiley-VCH, Weinheim, 2001), 675 pp).
19. (a) V. Wolf, Chem. Ber. 87 (1954) 668;
20. (b) J. Kaulen and H.J. Schäfer, Tetrahedron 38 (1982) 3299.
21. US patent 5 002 641 (Reilly Industries, Inc.) and references cited therein.
22. E. Steckhahn and C. Kandzia, Synlett (1992) 139.
23. R. DeClements and G.M. Swain, J. Electrochem. Soc. 144 (1997) 856.