Rapid simultaneous determination of amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine, 3,4-methylenedioxymethamphetamine, and 3,4-methylenedioxyethylamphetamine in urine by fast gas chromatography-mass spectrometry

Journal of Analytical Toxicology

Volumn 29, Issue 7, 2005, Pages 669-674

  Klette, Kevin L ^a   Jamerson, Matthew H ^a   Morris Kukoski, Cynthia L ^a,b   Kettle, Aaron R ^a   Snyder, J Jacob ^a  

^a Navy Drug Screening Laboratory   (United States)

^b Federal Bureau of Investigation   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

3,4 METHYLENEDIOXYAMPHETAMINE; 3,4 METHYLENEDIOXYETHYLAMPHETAMINE; 3,4 METHYLENEDIOXYMETHAMPHETAMINE; 4 CARBETHOXYHEXAFLUOROBUTYRYL CHLORIDE; AMPHETAMINE; AMPHETAMINE DERIVATIVE; CHLORIDE; EPHEDRINE; METHAMPHETAMINE; PERIODATE SODIUM; PHENTERMINE; PHENYLPROPANOLAMINE; PSEUDOEPHEDRINE; UNCLASSIFIED DRUG;

ANALYSIS; ANALYTIC METHOD; ARTICLE; CATION EXCHANGE; COMPARATIVE STUDY; CONTROLLED STUDY; DERIVATIZATION; DRUG DETERMINATION; DRUG URINE LEVEL; EXTRACTION; GAS CHROMATOGRAPHY; HUMAN; IMMUNOASSAY; MASS SPECTROMETRY; PRESSURE; SOLID PHASE EXTRACTION;

EID: 29144434016     PISSN: 01464760     EISSN: 01464760     Source Type: Journal    
DOI: 10.1093/jat/29.7.669     Document Type: Article

References (12)

1. U.S. Department of Health and Human Services, Substance Abuse and Mental Health Services Administration. Results from the 2001 National Household Survey on Drug Abuse: Volume I. Summary of National Findings. http://www.samhsa.gov/ oas/NHSDA/2k1NHSDA/vol1/Chapter5.htm, 2002.
2. M.J. Landry. MDMA: a review of epidemiologic data. J. Psychoactive Drugs 34: 163-169 (2002).
3. Office of the Department of Defense Coordinator for Drug Enforcement Policy and Support Memorandum. Drug Urinalysis Testing Levels, 1997.
4. Drug Detection Report, vol. 11. Business Publishers, Silver Spring, MD, 2001, p 126.
5. Federal Register 69(71): (2004).
6. P. Kintz, V. Cirimele, A. Traquo, and P. Mangin. Simultaneous determination of amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine and 3,4-methylenedioxymethamphetamine in human hair by GC/MS. J. Chromatogr. B 670: 162-166 (1995).
7. D. Hensley and J.T. Cody. Simultaneous determination of amphetamine, methamphetamine, methylenedioxyamphetamine (MDA), methylenedioxymethamphetamine (MDMA), and methylenedioxyethylamphetamine (MDEA) enantiomers by GC-MS. J. Anal. Toxicol. 23: 518-523 (1999).
8. P. Stout, C. Horn, and K. Klette. Rapid simultaneous determination of amphetamine (AMP), methamphetamine, 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymethamphetamine (MDMA), and 3,4-methylenedioxyethylamphetamine (MDEA) in urine by solid-phase extraction and GC-MS: a method optimized for high-volume laboratories. J. Anal. Toxicol. 26: 253-261 (2002).
9. F. Feyerherm and H. Prest. Fast GC/MS Methods for Routine Drug Analysis. Agilent Technologies. http://www.chem.agilent.com/temp/rad1E432/00015666.pdf, 1999.
10. Cerilliant Corporation, Analytical Reference Materials Custom Synthesis & Services Catalog, 2004.
11. M.A. ElSohly, D.F. Stanford, D. Sherman, H. Shah, D. Bernot, and C.E. Turner. A procedure for eliminating interferences from ephedra and related compounds in the GC/MS analysis of amphetamine and methamphetamine. J. Anal. Toxicol. 16: 109-111 (1992).
12. R.J. Czarny and C.L. Hornbeck. Quantitation of methamphetamine and amphetamine in urine by capillary GC/MS Part II. Derivitization with 4-carbethoxyhexafluorobutyryl chloride. J. Anal. Toxicol. 13: 257-262 (1989).