Measurement of coupling constants in symmetrical spin systems using a full multiple-step cross-polarization-driven NMR pulse scheme

Magnetic Resonance in Chemistry

Volumn 43, Issue 12, 2005, Pages 979-984

  Nolis, Pau ^a   Roglans, Anna ^b   Parella, Teodor ^a  

^a UNIVERSITAT AUTÒNOMA DE BARCELONA   (Spain)

^b UNIVERSITY OF GIRONA   (Spain)

Author keywords

Chemical equivalence; Heteronuclear cross polarization; Molecular symmetry; Proton carbon coupling constants; Proton proton coupling constants

Indexed keywords

CARBON;

CHEMICAL EQUIVALENCE; COUPLING CONSTANTS; CROSS POLARIZATIONS; HETERONUCLEAR CROSS-POLARIZATION; MEASUREMENTS OF; MOLECULAR SYMMETRY; PROTON-CARBON COUPLING CONSTANTS; PROTON-PROTON COUPLING CONSTANTS; SPIN SYSTEMS; SPIN-S SYSTEMS;

POLARIZATION;

EID: 28644434550     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.1670     Document Type: Article

References (21)

1. (a) Radeglia R, Poleschner H, Heydenreich M. Magn. Reson. Chem. 1991; 29: 1028;
2. (b) Buevich AV, Chan T, Wang CH, McPhail AT, Ganguly AK. Magn. Reson. Chem. 2005; 43: 187.
3. Mucci A, Parenti F, Schenetti L. Eur. J. Org. Chem. 2002; 938.
4. Luy B, Hauser G, Kirschning A, Glaser SJ. Angew. Chem. Int. Ed. 2003; 42: 1300.
5. Fäcke T, Berger S. J. Magn. Reson. A 1995; 113: 114.
6. Nolis P, Roglans A, Parella T. J. Magn. Reson. 2005; 173: 305.
7. (a) Parella T. J. Magn. Reson 2004; 167: 266;
8. (b) Luy B. J. Magn. Reson. 2004; 168: 210.
9. (a) Chiarparin E, Pelupessy P, Bodenhausen G. Mol. Phys. 1998; 95: 759;
10. (b) Pelupessy P, Chiarparin E. Conc. Magn. Reson. 2000; 12: 103.
11. Parella T, Belloc J, Sánchez-Ferrando F. Magn. Reson. Chem. 2004; 42: 852.
12. (a) Willker W, Leibfritz D. J. Magn. Reson. 1992; 99: 421;
13. (b) Sorensen MD, Meissner A, Sorensen OW. J. Magn. Reson. 1999; 137: 237.
14. (a) Sorensen MD, Meissner A, Sorensen OW. J. Biomol. NMR 1997; 10: 181;
15. (b) Meissner A, Duus JO, Sorensen OW. J. Magn. Reson. 1997; 128: 92;
16. (c) Meissner A, Duus JO, Sorensen OW. J. Biomol. NMR 1997; 10: 89.
17. Luy B, Barchi JJ, Marino JP. J. Magn. Reson. 2001; 152: 179.
18. Peti W, Griesinger C. J. Am. Chem. Soc. 2000; 122: 3975.
19. (a) Parella T. J. Biomol. NMR 2004; 29: 37;
20. (b) Parella T, Gairí M. J. Am. Chem. Soc. 2004; 126: 9821.
21. Torrent A, González I, Pla-Quintana A, Roglans A, Moreno-Mañas M, Parella T, Benet-Buchholz J. J. Org. Chem. 2005; 70: 2033.