Non-aqueous capillary electrophoresis for separation and simultaneous determination of fraxin, esculin and esculetin in Cortex fraxini and its medicinal preparations

Biomedical Chromatography

Volumn 19, Issue 9, 2005, Pages 696-702

  Li, Cunhong ^a,b   Chen, Anjia ^a,c   Chen, Xiaofeng ^a   Ma, Xiao ^d   Chen, Xingguo ^a   Hu, Zhide ^a  

^a LANZHOU UNIVERSITY   (China)

^b JIAOZUO UNIVERSITY   (China)

^c SHANXI AGRICULTURAL UNIVERSITY   (China)

^d Gansu Provincial Institute for Drug Control   (China)

Author keywords

Esculetin; Esculin; Fraxin; Non aqueous capillary electrophoresis

Indexed keywords

CAPILLARY ELECTROPHORESIS;

ANALYTES; CORTEX FRAXINUS; ESCULETIN; ESCULIN; FRAXIN; FUSED-SILICA CAPILLARIES; MEDICINAL PREPARATION; NON-AQUEOUS CAPILLARY ELECTROPHORESIS; PEAK HEIGHT; SIMULTANEOUS DETERMINATIONS;

FUSED SILICA;

ACETIC ACID; ACETONITRILE; AMMONIUM ACETATE; BAI TOU WENG TANG; BUFFER; CHINESE DRUG; CHOLIC ACID; ESCULETIN; ESCULIN; FRAXIN; FRAXINUS EXTRACT; PLANT EXTRACT; UNCLASSIFIED DRUG;

ARTICLE; BARK; CALIBRATION; CAPILLARY ELECTROPHORESIS; CHINESE HERB; CORRELATION COEFFICIENT; DRUG DETERMINATION; DRUG ISOLATION; DRUG STRUCTURE; FRAXINUS; NONHUMAN; REPRODUCIBILITY; SEPARATION TECHNIQUE; STRUCTURE ANALYSIS;

FRAXINUS;

EID: 28444464397     PISSN: 02693879     EISSN: None     Source Type: Journal    
DOI: 10.1002/bmc.497     Document Type: Article

References (30)

1. Chen AJ, Zhang JY, Chen XF, Hu ZD and Chen XG. Separation and determination of active components in Radix Salviae miltiorrhizae and its medicinal preparations by nonaqueous capillary electrophoresis. Journal of Separation Science 2004; 27: 569-575.
2. Chu CY, Tsai YY, Wang CJ, Lin WL and Tseng TH. Induction of apoptosis by esculetin in human leukemia cells. European Journal of Pharmacology 2001; 416: 25-32.
3. Duncan SH, Flint HJ and Stewart CS. Inhibitory activity of gut bacteria against Escherichia coil O157 mediated by dietary plant metabolites. FEMS Microbiology Letters 1998; 164: 283-288.
4. Fillet M, Servais AC and Crommen J. Effects of background electrolyte composition and addition of selectors on separation selectivity in nonaqueous capillary electrophoresis. Electrophoresis 2003; 24: 1499-1507.
5. Grob M and Steiner F. Application of nonaqueous capillary electrophoresis to the simultaneous analysis of anionic surfactants. Electrophoresis 2002a; 23: 1921-1927.
6. Grob M and Steiner F. Characteristics of the electroosmotic flow of electrolyte systems for nonaqueous capillary electrophoresis. Electrophoresis 2002b; 23: 1853-1861.
7. Huang Y. Clinical application of Bai-tou-weng-tang. Zhongchengyao 1995; 17: 35-36.
8. Ji S and Wang K. Determination of fraxelin A and fraxetin B Cortex Fraxini by HPLC. Zhongcheng Yao 1997; 19: 40-41.
9. Li L, Yuan B, Lan YQ and Cao Y. Determination of aesculin in Fufang Qinpi Guangtangji. Zhongguo Linchuang Yaoxue Zazhi 2002; 11: 296-298.
10. Li YQ, Cui SY, Cheng YQ, Chen XG and Hu ZD. Application of nonaqueous capillary electrophoresis for quantitative analysis of quinolizidine alkaloids in Chinese herbs. Analytica Chimica Acta 2004; 508: 17-22.
11. Ochocka RJ, Rajzer D, Kowalski P and Lamparczyk H. Determination of coumarins from Chrysanthemum segetum by capillary electrophoresis. Journal of Chromatography A 1995; 709: 197-202.
12. Pu XF, Ling XQ and Zhuang XH. Quality evaluation of Contex fraxini. Huaxi Yaoxue Zazhi 2001; 17: 4-6.
13. Qiu ZY and Xin XQ. Quantitative determination of the content of esculetin in Fulinkang by HPLC. Shenyang Yaoke Daxue Xuebao 2000; 17: 347-348.
14. Ran L, Zeng Y, Chao RB and Wu J. Determination of aesculin and aesculetin in Xitongning capsule by HPLC. Huaxi Yaoxue Zazhi 2001; 16: 135-136.
15. Riekkola ML. Recent advances in nonaqueous capillary electrophoresis. Electrophoresis 2002; 23: 3865-3883.
16. Riekkola ML, Jussila M, Porras SP and Valko IE. Non-aqueous capillary electrophoresis. Journal of Chromatography A 2000; 892: 155-170.
17. Song JZ, Xu HX, Tian SJ and But PPH. Determination of quinolizidine alkaloids in traditional Chinese herbal drugs by nonaqueous capillary electrophoresis. Journal of Chromatography A 1999; 857: 303-311.
18. Stefanova Z, Neychev H, Ivanovska N and Kostova I. Effect of a total extract from Fraxinus ornus stem bark and esculin on zymosan- and carrgeenan-induced paw oedema in mice. Journal of Ethnopharmacology 1995; 46: 101-106.
19. Steiner F and Hassel M. Nonaqueous capillary electrophoresis: a versatile completion of electrophoretic separation techniques. Electrophoresis 2000; 21: 3994-4016.
20. Wang CJ, Hsieh YJ, Chu CY, Lin YL and Tseng TH. Inhibition of cell cycle progression in human leukemia HL-60 cells by esculin. Cancer Letters 2002; 183: 163-168.
21. Wang X, Zhang X, Zhao HP and Zhang XQ. Determination of aesculetin in Qinpi by HPLC. Zhongguo Shiyan Fangjixue Zazhi 2004; 10: 6-7.
22. Xiao PG, Li DP and Yang SL. Modern Chinese Materica Media, Vol. 3. Chemistry Industry Publisher, Beijing, China; 2002; 633.
23. Xu HB. Determination of aesculin and aesculetin in Qinpi extracts by HPLC. Xiandai Zhongyao Yanjiu Yu Shijian 2003; 17: 41-42.
24. Yang TM, Ge X and Wang XN. Study of antibacterial function of Contex fraxini. Xibei Guofang Yixue Zazhi 2003; 24: 387-388.
25. You TY, Yang XR and Wang EK. End-column amperometric detection of aesculin and aesculetin by capillary electrophoresis. Analytica Chimica Acta 1999; 401: 29-34.
26. Zarbl E, Lammerhofer M, Franco P, Petracs M and Linder W. Delelopment of stereoselective nonaqueous capillary system for the resolution of cationic and amphoteric analytes. Electrophoresis 2001; 22: 3297-3307.
27. Zhang HY, Li QF, Shi ZH, Hu ZD and Wang R. Analysis of aesculin and aesculetin in Cortex forxini by capillary zone electrophoresis. Talanta 2000; 52: 607-621.
28. Zhao SG, Pan ZW, Chen XG and Hu ZD. Analysis of the aconitine alkaloids in traditional Chinese medicines by nonaqueous capillary electrophoresis using a new recording mode. Biomedical Chromatography 2004; 18: 381-387.
29. Zhu XX, Peng DH, Tao Y, Chen XB and Qiu ZJ. Determination of aesculin in AB-Yanmo by TLC. Nanjing Zhongyiyao Daxue Xuebao 1998; 14: 158.
30. Zuo YM, Wang ZY, Cui HH and Liu LM. Determination of aesculin and aesculetin in periderm and leaves of Cortex fraxini among different provenances. Zhongcheng Yao 2003; 25: 552-554.