An asymmetric synthesis of (+)-cryptone

Synthetic Communications

Volumn 20, Issue 8, 1990, Pages 1159-1165

  Hawley, Ronald C ^a   Schreiber, Stuart L ^a  

^a YALE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 28444454800     PISSN: 00397911     EISSN: 15322432     Source Type: Journal    
DOI: 10.1080/00397919008052823     Document Type: Article

References (10)

1. Current address: Department of Chemistry, Harvard University, 12 Oxford St., Cambridge, MA 02138
2. Schreiber, S.L.; Hawley, R.C. Tetrahedron Lett., 1985, 26, 5971.
3. Schreiber, S.L.; Santini, C. J. Am. Chem. Soc., 1984, 106, 4038.
4. 4. Atomic coordinates for 2 and 3 have been deposited in the Cambridge Structural Database. We thank Gayle Schulte (Yale Chemical Instrumentation Center) for performing these analyses.
5. Brown, H.C.; Singaram, B.J. J. Am. Chem. Soc. 1984, 106, 1797.
6. Dale, J.A.; Dull, D.L.; Mosher, H.S. J. Org. Chem. 1969, 34, 2543.
7. Soffer, M.D.; Gunay, G.E.; Korman, O.; Adams, M.B. Tetrahedron Lett. 1963, 389.
8. 8. For a recent asymmetric synthesis of (+)- 1 in 66% ee, see: R. Shirai, R.; Tanaka, M.; Koga, K. J. Am. Chem. Soc. 1986,108, 543.
9. 9. For a recent example of the use of (+)-1 (prepared by the method described in ref 8) in natural products synthesis, see: Greene, A. E.; Serra, A. A.; Barreiro, E. J.; Costa, P. R. R. J. Org. Chem. 1987, 52, 1169.
10. 10. Still, W.C.; Kahn, M.; Mitra, A. J. Org. Chem. 1978, 43, 2923.