Asymmetric catalytic hydrogenations at micro-litre scale in a helicoidal single channel falling film micro-reactor

Catalysis Today

Volumn 110, Issue 1-2, 2005, Pages 179-187

  De Bellefon, C ^a   Lamouille, T ^a   Pestre, N ^a   Bornette, F ^a   Pennemann, H ^b   Neumann, F ^b   Hessel, V ^b  

^a CNRS   (France)

^b INSTITUT FÜR MIKROTECHNIK MAINZ GMBH   (Germany)

Author keywords

Asymmetric catalysis; Catalyst screening; Homogeneous catalysis; Kinetic; Micro reactors

Indexed keywords

CATALYSTS; CHEMICAL REACTORS; METHANOL; SOLVENTS; VISCOSITY;

CATALYST SCREENING; HOMOGENEOUS CATALYSIS; KINETIC; MICRO-REACTORS;

HYDROGENATION;

EID: 27744505154     PISSN: 09205861     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cattod.2005.09.002     Document Type: Article

References (26)

1. V. Hessel, S. Hardt, and H. Löwe Chemical Micro-process Engineering: Fundamentals 2004 Wiley-VCH Weinheim
2. P.D.I. Fletcher, S.J. Haswell, E. Pombo-Villar, B.H. Warrington, P. Watts, S.Y.F. Wong, and H. Zhang Micro-reactors: principles and applications in organic synthesis Tetrahedron 58 2002 4735
3. A. Gravilidis, P. Angeli, E. Cao, K.K. Yeong, and Y.S.S. Wan Technology and applications of micro-engineered reactors Chem. Eng. Res. Des. 80 2002 3
4. K. Jähnisch, V. Hessel, H. Löwe, and M. Baerns Chemistry in micro-structured reactors Angew. Chem. Int. Ed. 43 2004 406
5. K.F. Jensen Micro-reaction engineering - is small better? Chem. Eng. Sci. 56 2001 293 303
6. E.V. Rebrov, S.A. Duinkerke, M.H.J.M. de Croon, and J.C. Schouten Optimization of heat transfer characteristics, flow distribution, and reaction processing for a micro-structured reactor/heat-exchanger for optimal performance in platinum catalyzed ammonia oxidation Chem. Eng. J. 93 2003 201 216 (and references cited therein)
7. A. Rouge, B. Spoetzl, K. Gebauer, R. Schenk, and A. Renken Micro-channel reactors for fast periodic operation: the catalytic dehydration of isopropanol Chem. Eng. Sci. 56 2001 1419 1427
8. C. de Bellefon, N. Tanchoux, S. Caravieilhes, P. Grenouillet, and V. Hessel Angew. Chem. Int. Ed. 39 2000 3442
9. C. de Bellefon, R. Abdallah, T. Lamouille, N. Pestre, S. Caravieilhes, and P. Grenouillet High troughput screening of molecular catalysts using automated liquid handling, injection and micro-devices Chimia 56 2002 621 626
10. R. Abdallah, V. Meille, J. Shaw, D. Wenn, and C. de Bellefon Gas-liquid and gas-liquid-solid catalysis in a mesh micro-reactor Chem. Commun. 2004 372
11. S.K. Ajmera, C. Delattre, M. Schmidt, and K.F. Jensen Micro-fabricated differential reactor for heterogeneous gas phase catalyst testing J. Catal. 209 2002 401 412
12. C. de Bellefon, N. Pestre, T. Lamouille, P. Grenouillet, and V. Hessel Adv. Synth. Catal. 345 2003 190
13. V. Hessel, H. Löwe, A. Müller, and G. Kolb Chemical Micro-process Engineering: Processing and Plants 2005 Wiley-VCH Weinheim
14. M.G. Pollack, R.B. Fairb, and A.D. Shenderov Electrowetting-based actuation of liquid droplets for micro-fluidic applications Appl. Phys. Lett. 77 2000 1725 1726
15. K. Jahnisch, M. Baerns, V. Hessel, W. Ehrfeld, V. Haverkamp, H. Lowe, Ch. Wille, and A. Guber J. Fluorine Chem. 105 2000 117
16. Micro-bubble Beam (MBB) A potential dispersion mechanism for multiphase gas-liquid micro-reactor systems Doku George N Ind. Eng. Chem. Res. 42 2003 3721 3730
17. S. Hardt, T. Dietrich, A. Freitag, V. Hessel, H. Löwe, C. Hofmann, A. Oroskar, F. Schönfeld, and K. Vanden Bussche Radial and tangential injection of liquid/liquid and gas/liquid streams and focusing thereof in a special cyclone mixer Proceedings of the Sixth International Conference on Micro-reaction Technology IMRET 6 AIChE Pub. No. 164: New Orleans, USA, 2002 2002 329 344
18. N. de Mas, A. Guenther, M.A. Schmidt, and K.F. Jensen Micro-fabricated multiphase reactors for the selective direct fluorination of aromatics Ind. Eng. Chem. Res. 42 2003 698
19. M.W. Losey, M.A. Schmidt, and K.F. Jensen Micro-fabricated multiphase packed-bed reactors: characterization of mass transfer and reactions Ind. Eng. Chem. Res. 40 2001 2555
20. J. Kobayashi, Y. Mori, K. Okamoto, R. Akiyama, M. Ueno, T. Kitamori, and S. Kobayashi A micro-fluidic device for conducting gas-liquid-solid hydrogenation reactions Science 304 2004 1305 1308
21. K.-K. Yeong, A. Gavriilidis, R. Zapf, and V. Hessel Catalyst preparation and deactivation issues for nitrobenzene hydrogenation in a micro-structured falling film reactor Catal. Today 81 2003 641
22. R.D. Chambers, D. Holling, A.J. Rees, and G. Sandford Micro-reactors for oxidations using fluorine J. Fluorine Chem. 119 2003 81 82 (and references cited therein)
23. E.N. Jacobsen A. Pfaltz H. Yamamoto Handbook of Asymmetric Catalysis 2000 Springer (many examples can be, found)
24. R. Noyori Asymmetric Catalysis in Organic Synthesis 1994 Wiley New York
25. V. Meille, N. Pestre, P. Fongarland, and C. de Bellefon Gas-liquid mass transfer in small laboratory batch reactors: comparison of methods Ind. Chem. Eng. Res. 43 2004 924 927
26. N. Pestre, PhD thesis, Université Claude Bernard de Lyon, 2004.