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21
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27644511744
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note
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2O ligands where unresolved residual density suggests some slight disorder between the ligands. The fact that this could not be successfully modelled is reflected in the rather high residuals. CCDC 273243 (2b), 273246 (3) and 273245 (4). See http:// dx.doi.org/10.1039/ b509310d for crystallographic data in CIF or other electronic format..
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22
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0031231813
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Seifert, T.8
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23
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27644566218
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note
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2, SHELX-97. H atoms were omitted.
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-
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24
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0141757432
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25
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26
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27644578119
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note
-
4] with the trigonal pyramids aligned; in either case the arrangement is then disordered so as to average the structure. These THF ligands are of course also disordered about the 3-fold axis.
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27
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27644537099
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EPR-measurement and simulation: D. M. Murphy at the EPSRC National ENDOR Service, Cardiff University, UK
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EPR-measurement and simulation: D. M. Murphy at the EPSRC National ENDOR Service, Cardiff University, UK.
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28
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0033785793
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