Three piperazine complexes of divalent mercury: Hg(CF3) 2(Pip), Hg(SCN)2(Pip), and (Hg(SCN)2) 2(Pip)

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 631, Issue 13-14, 2005, Pages 2923-2927

  Nolte, Matthias ^a   Pantenburg, Ingo ^a   Meyer, Gerd ^a  

^a UNIVERSITY OF COLOGNE   (Germany)

Author keywords

Bis(trifluoromethyl)mercury; Crystal Structure; Mercuric thiocyanate; Mercury; Piperazine

Indexed keywords

EID: 27644543171     PISSN: 00442313     EISSN: None     Source Type: Journal    
DOI: 10.1002/zaac.200500280     Document Type: Article

References (21)

1. For a recent review see: D. K. Breitinger, Cadmium and Mercury, in: Comprehensive Coordination Chemistry II (J. A. McCleverty, T. J. Meyer, editors-in-chief), Vol. 6 (D. E. Fenton, volume editor), chapter 6.9, 1253-1292, Elsevier (2004).
2. G. Meyer, P. Nockemann, Z. Anorg. Allg. Chem. 2003, 629, 1447.
3. 2 (X = Cl, Br, I): D. Grdenic, I. Krstanovic, Arkhiv Khem. 1955, 27, 143;
4. P. Nockemann, Dissertation, Universität zu Köln, 2002.
5. 2: P. Nockemann, Dissertation, Universität zu Köln, 2002.
6. 2(Pyo): P. Nockemann, G. Meyer, Acta Crystallogr. 2004, E60. m751;
7. 2(Pyo): P. Nockemann, G. Meyer, Acta Crystallogr. 2004, E60, m753;
8. 2(Pym) (X = Cl, Br): P. Nockemann. Dissertation, Universität zu Köln, 2002;
9. 2(Pyp): P. Nockemann, G. Meyer, Acta Crystallogr. 2004, E60, m744;
10. 2: P. Nockemann, G. Meyer, Acta Crystallogr. 2004, E60, m747;
11. 2(Pyp): P. Nockemann, G. Meyer, Acta Crystallogr. 2004, E60, m749 .
12. P. Nockemann, F. Schulz, D. Naumann, G. Meyer, Z. Anorg. Allg. Chem. 2005, 631, 649.
13. M. Nolte, Staatsexamensarbeit, Universität zu Köln 2003;
14. M. Nolte, Dissertation, Universität zu Köln, 2004.
15. W. A. Herrmann, G. Brauer, Synthetic methods of organometallic and inorganic chemistry, Vol. 5, G. Thieme, Stuttgart 1999, S. 221.
16. Structure solutions and refinements were performed with the programs SHELXS-97 and SHELXL-97 (G. M. Sheldrick, Göttingen).
17. Scattering factors were taken from International Tables for X-ray Crystallography, Vol C. Absorption was corrected numerically with the aid of the programs X-RED and X-SHAPE (Stoe, Darmstadt, 1994). Crystallographic data for the structures have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC 274130 for (1), CCDC 274129 for (2), and CCDC 274131 for (3). Copies of the data can be obtained, free of charge, on application to CHGC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: +44 1223 336033 or e-mail: deposit@ccdc.cam.ac.uk).
18. D. J. Brauer, H. Bürger, R. Eujen, J. Organomet. Chem. 1977, 135, 281.
19. A. L. Beauchamp, D. Goutier, Can. J. Chem. 1972, 50, 977.
20. P. Nockemann, A.-V. Mudring, G. Meyer, to be published.
21. P. Nockemann, Dissertation, Universität zu Köln, 2002.