Development and application of HPLC methods with tandem mass spectrometric detection for the determination of hydrochlorothiazide in human plasma and urine using 96-well liquid-liquid extraction

Journal of Liquid Chromatography and Related Technologies

Volumn 28, Issue 17, 2005, Pages 2681-2703

  Fang, W ^a   Xie, W ^a   Hsieh, J Y K ^a   Matuszewski, B K ^a  

^a MERCK RESEARCH LABORATORIES   (United States)

Author keywords

96 Well liquid liquid extraction; HPLC MS MS determination; Human plasma; Hydrochlorothiazide; Hydroflumethiazide; Urine

Indexed keywords

BODY FLUIDS; CHLORINE COMPOUNDS; DRUG PRODUCTS; EXTRACTION; MASS SPECTROMETRY; PHARMACOKINETICS;

96-WELL LIQUID-LIQUID INTERACTION; HPLC-MS/MS DETERMINATION; HUMAN PLASMA; HYDROCHLOROTHIAZIDE; HYDROFLUMETHIAZIDE; URINE;

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

2 BUTYL 4 CHLORO 1 [[2' (1H TETRAZOL 5 YL) 4 BIPHENYLYL]METHYL] 5 IMIDAZOLECARBOXYLIC ACID; HYDROCHLOROTHIAZIDE; HYDROCHLOROTHIAZIDE PLUS LOSARTAN; HYDROFLUMETHIAZIDE; LOSARTAN POTASSIUM;

ACCURACY; ARTICLE; BIOEQUIVALENCE; COMPUTER PROGRAM; CONTROLLED STUDY; DRUG DETERMINATION; DRUG ISOLATION; DRUG STRUCTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; IONIZATION; LIQUID LIQUID EXTRACTION; MASS SPECTROMETER; PLASMA; REPRODUCIBILITY; ROBOTICS; STANDARD; TANDEM MASS SPECTROMETRY; URINE LEVEL; VALIDATION PROCESS;

EID: 27544461967     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070500224666     Document Type: Article

References (22)

1. Miller, R.; Amestoy, C. A liquid chromatographic method for the determination of hydrochlorothiazide in human plasma. J. Pharm. Biomed. Anal. 1992, 10, 541-545.
2. Ulvi, V.; Keski-Hynnila, H. First-derivative UV spectrophotometric and high-performance liquid chromatographic analysis of some thiazide diuretics in the presence of their photodecomposition products. J. Pharm. Biomed. Anal. 1994, 12, 917-922.
3. Warily, A.F.; Belal, S.F.; Heaba, E.A.; Kersh, A.E. Simultaneous determination of enalapril maleate and hydrochlorothiazide by first-derivative ultraviolet spectrophotometry and high-performance liquid chromatography. J. Pharm. Biomed. Anal. 1995, 13, 851-856.
4. Gilliard, J.A.; Ritter, C. Use of simulated liquid chromatography-diode array detection data for the definition of a guide curve in peak purity assessment by spectral comparison. J. Chromatogr. A. 1997, 786, 1-11.
5. Farthing, D.; Fakhry, I.; Ripley, E.B.; Sica, D. Simple method for determination of hydrochlorothiazide in human urine by high performance liquid chromatography utilizing narrowbore chromatography. J. Pharm. Biomed. Anal. 1998, 17, 1455-1459.
6. Panderi, I.E.; Parissi-Poulou, M. Simultaneous determination of benazepril hydrochloride and hydrochlorothiazide by micro-bore liquid chromatography. J. Pharm. Biomed. Anal. 1999, 21, 1017-1024.
7. Carlucci, G.; Palumbo, G.; Mazzeo, P.; Quaglia, M.G. Simultaneous determination of losartan and hydrochlorothiazide in tablets by high-performance liquid chromatography. J. Pharm. Biomed. Anal. 2000, 23, 185-189.
8. Dine, E.; Baleanu, D. Spectrophotometric quantitative determination of cilazapril and hydrochlorothiazide in tablets by chemometric methods. J. Pharm. Biomed. Anal. 2002, 30, 715-723.
9. Hertzog, D.L.; McCafferty, J.F.; Fang, X.; Tyrrell, R.J.; Reed, R.A. Development and validation of a stability-indicating HPLC method for the simultaneous determination of Losartan potassium, hydrochlorothiazide, and their degradation products. J. Pharm. Biomed. Anal. 2002, 30, 747-760.
10. Erturk, S.; Cetin, S.M.; Atmaca, S. Simultaneous determination of moexipril hydrochloride and hydrochlorothiazide in tablets by derivative spectrophotometric and high-performance liquid chromatographic methods. J. Pharm. Biomed. Anal. 2003, 33, 505-511.
11. Erk, N. Simultaneous determination of irbesartan and hydrochlorothiazide in human plasma by liquid chromatography. J. Chromatogr. B 2003, 784, 195-201.
12. Zendelovska, D.; Stafilov, T.; Milosevski, P. Development of solid-phase extraction method and its application for determination of hydrochlorothiazide in human plasma using HPLC. Biomed. Chromatogr. 2004, 18, 71-76.
13. Hsieh, J.Y.-K.; Lin, C.; Matuszewski, B.K.; Dobrinska, M.R. Fully automated methods for the determination of hydrochlorothiazide in human plasma and urine. J. Pharm. Biomed. Anal. 1994, 12, 1555-1562.
14. Foltea, M.; Simard, M.; Gauthier-Dubois, G.; Fragiskatos, O. A rapid, sensitive and specific negative ion mode LC/MS/MS method for the determination of hydrochlorothiazide in human plasma. In: Proceedings of the 49th ASMS Conference on Mass Spectrometry and Allied Topics, Chicago, IL, 2001, Poster 1059.
15. Takubo, T.; Okada, H.; Ishii, M.; Hara, K.; Ishii, Y. Sensitive and selective liquid chromatography-electrospray ionization tandem mass spectrometry analysis of hydrochlorothiazide in rat plasma. J. Chromatogr. B 2004, 806, 199-203.
16. Matuszewski, B.K.; Constanzer, M.L.; Chavez-Eng, C.M. Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLC-MS/MS. Anal. Chem. 2003, 75, 3019-3030.
17. Rose, M.J.; Merschman, S.A.; Eisenhandler, R.; Woolf, E.J.; Yeh, K.C.; Lin, L.; Fang, W.; Hsieh, J.; Braun, M.P.; Gatto, G.J.; Matuszewski, B.K. High-throughput simultaneous determination of the HIV protease inhibitors indinavir and L-756423 in human plasma using semi-automated 96-well solid phase extraction and LC-MS/MS. J. Pharm. Biomed. Anal. 2000, 24, 291-305.
18. Matthews, C.Z.; Woolf, E.J.; Matuszewski, B.K. Improved procedure for the determination of rofecoxib in human plasma involving 96-well solid-phase extraction and fluorescence detection. J. Chromatogr. A 2002, 949, 83-89.
19. Xue, L.L.; Lin, L.; Hsieh, J.Y.-K.; Matuszewski, B.K. Determination of a selective GABA-A 5 receptor inverse agonist in human plasma by high-performance liquid chromatography with tandem mass spectrometric detection. J. Liq. Chromatogr. & Rel. Technol. 2004, 27, 689-704.
20. Hsieh, J.Y.-K.; Lin, L.; Matuszewski, B.K. A semi-automated 96-well solid phase extraction and high performance liquid chromatographic determination of a selective GABA-A receptor agonist in human and rat plasma using fluorescence detection. J. Liq. Chromatogr. & Rel. Technol. 2004, 27, 2329-2341.
21. Popot, M.A.; Garcia, P.; Fournier, F.; Bonnaire, Y.; Tabet, J.C. Gas-phase behaviour of negative ions produced from thiazidic diuretics under electrospray conditions. J. Mass. Spectrom. 2002, 37, 940-953.
22. Matuszewski, B.K.; Chavez-Eng, C.M.; Constanzer, M.L. Development of high-performance liquid chromatography-tandem mass spectrometric methods for determination of new oxytocin receptor antagonist (L-368,899) extracted from human plasma and urine: a case of lack of specificity due to the presence of metabolites. J. Chromatogr. B 1998, 716, 195-208.