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17
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27144556862
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note
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3 ligands (see ref 11).
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18
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42649139656
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Sénèque, O.; Rondelez, Y.; Le Clainche, L.; Inisan, C.; Rager, M.-N.; Giorgi, M.; Reinaud, O. Eur. J. Inorg. Chem. 2001, 2597.
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Inisan, C.4
Rager, M.-N.5
Giorgi, M.6
Reinaud, O.7
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19
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85045721735
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20
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27144457274
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-
note
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3 with only a few molar equivalents of MeCN.
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-
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21
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27144474380
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note
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2O and MeOH are good donors but lack a lipophilic chain. Therefore, they are not "good" guests (see refs 7, 8).
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22
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27144492538
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note
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An associative mechanism implying the coordination of a sixth ligand to zinc is highly unlikely, due to sterical overcrowding at the metal center in such an environment.
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25
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33745231055
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Orpen, A. G.; Brammer, L.; Allen, F. H.; Kennard, O.; Watson, D. G.; Taylor, R. J. Chem. Soc., Dalton. Trans. 1989, S1.
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Kennard, O.4
Watson, D.G.5
Taylor, R.6
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27
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0037415433
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A rare example has been recently reported. See: Akine, S.; Goto, K.; Kawashima, T. Tetrahedron Lett. 2003, 44, 1171.
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Akine, S.1
Goto, K.2
Kawashima, T.3
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28
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0003894828
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Stoddart, J. F., Ed.; The Royal Society of Chemistry: Cambridge, U.K.
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Gutsche, C. D. In Calixarenes, Monographs in Supramolecular Chemistry; Stoddart, J. F., Ed.; The Royal Society of Chemistry: Cambridge, U.K., 1989.
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Gutsche, C.D.1
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29
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85046911837
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The self-inclusion of one imidazole unit into the calix[6]cavity has been previously observed in a tetranuclear Cu(II) complex that was characterized by X-ray diffraction analysis. Sénèque, O.; Campion, M.; Douziech, B.; Giorgi, M.; Rivière, E.; Journaux, Y.; Le Mest, Y.; Reinaud, O. Eur. J. Inorg. Chem. 2002, 2007.
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Sénèque, O.1
Campion, M.2
Douziech, B.3
Giorgi, M.4
Rivière, E.5
Journaux, Y.6
Le Mest, Y.7
Reinaud, O.8
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30
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85083119867
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This has also been observed with other calixarene-based complexes. See, for example: Darbost, U.; Zeng, X.; Rager, M.-N.; Giorgi, M.; Jabin, I.; Reinaud, O. Eur. J. Inorg. Chem. 2004, 4371.
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Darbost, U.1
Zeng, X.2
Rager, M.-N.3
Giorgi, M.4
Jabin, I.5
Reinaud, O.6
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31
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27144460447
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Engendilger, E.; Armspach, D.; Matt, D. Chem. Rev. 2004, 104, 4147.
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Engendilger, E.1
Armspach, D.2
Matt, D.3
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32
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27144481874
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note
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Finally, in our proposed catalytic cycle, inactivation of the enzyme at low pH could stem from the protonation of the glutamate residue.
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-
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33
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27144453232
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note
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Such a mechanism cannot be efficient in our calixarene-based system as the narrow rim of the macrocycle precludes the stabilization of a tetrahedral intermediate in the endo-position for sterical reasons.
-
-
-
-
34
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27144548719
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note
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2] = 0.2124. See Table S1 in the Supporting Information.
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